C₆₈H₁₁₀N₆O₁₅Si₄

Base Information

Chemical Name:C₆₈H₁₁₀N₆O₁₅Si₄
CAS No.:1579198-25-6
Molecular Formula:C₆₈H₁₁₀N₆O₁₅Si₄
Molecular Weight:1363.99
Hs Code.:

C<sub>68</sub>H<sub>110</sub>N<sub>6</sub>O<sub>15</sub>Si<sub>4</sub>

Synonyms:C₆₈H₁₁₀N₆O₁₅Si₄

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Chemical Property of C₆₈H₁₁₀N₆O₁₅Si₄

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Technology Process of C₆₈H₁₁₀N₆O₁₅Si₄

There total 16 articles about C₆₈H₁₁₀N₆O₁₅Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 2-O-benzoyl-3,4-di-O-methyl-D-rhamnopyranosyl ortho-cyclopropylethynylbenzoate

: 1579198-23-4
C₅₃H₉₂N₆O₁₀Si₄

: 1579198-25-6
C₆₈H₁₁₀N₆O₁₅Si₄

Guidance literature:: 2-O-benzoyl-3,4-di-O-methyl-D-rhamnopyranosyl ortho-cyclopropylethynylbenzoate; C₅₃H₉₂N₆O₁₀Si₄; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere; Molecular sieve;

With trifluoromethanesulfonyloxy(triphenylphosphine)gold(I); In dichloromethane; at 0 ℃; for 1.5h; Inert atmosphere; Molecular sieve;
DOI:10.1021/ja501460j

Reference yield:

: 1579198-10-9
C₃₁H₂₅N₃O₇

: 1579198-25-6
C₆₈H₁₁₀N₆O₁₅Si₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve

1.2: 2 h / Inert atmosphere; Molecular sieve

2.1: ethanol; water / 8 h / 20 - 90 °C / Inert atmosphere

3.1: pyridine / 1.5 h / 20 °C / Inert atmosphere

4.1: triphenylphosphine; silica gel; water / tetrahydrofuran / 4 h / 20 - 50 °C / Inert atmosphere

5.1: N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

6.1: triethylamine / dichloromethane / 5 h / 20 °C / Inert atmosphere

7.1: lithium borohydride / tetrahydrofuran / -40 - 20 °C / Inert atmosphere

8.1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve

8.2: 1.5 h / 0 °C / Inert atmosphere; Molecular sieve

With pyridine; lithium borohydride; water; silica gel; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja501460j

Reference yield:

: 1579198-21-2
C₄₂H₆₄N₆O₁₁Si₂

: 1579198-25-6
C₆₈H₁₁₀N₆O₁₅Si₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 5 h / 20 °C / Inert atmosphere

2.1: lithium borohydride / tetrahydrofuran / -40 - 20 °C / Inert atmosphere

3.1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve

3.2: 1.5 h / 0 °C / Inert atmosphere; Molecular sieve

With lithium borohydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja501460j