Technology Process of C45H82O5Si4
There total 7 articles about C45H82O5Si4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C45H84O5Si4;
With
oxalyl dichloride; dimethyl sulfoxide;
at -78 ℃;
With
triethylamine;
DOI:10.1055/s-0030-1260586
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridinium p-toluenesulfonate / tetrahydrofuran / 20 °C
2: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane
3: water; acetic acid / 1.5 h / 20 °C
4: 2,6-dimethylpyridine / dichloromethane / 2.5 h / -15 - 0 °C
5: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 24 h / 20 °C
6: oxalyl dichloride; dimethyl sulfoxide / -78 °C
With
2,6-dimethylpyridine; oxalyl dichloride; 20 % Pd(OH)2/C; water; hydrogen; pyridinium p-toluenesulfonate; acetic acid; dimethyl sulfoxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1055/s-0030-1260586
- Guidance literature:
-
Multi-step reaction with 4 steps
1: water; acetic acid / 1.5 h / 20 °C
2: 2,6-dimethylpyridine / dichloromethane / 2.5 h / -15 - 0 °C
3: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 24 h / 20 °C
4: oxalyl dichloride; dimethyl sulfoxide / -78 °C
With
2,6-dimethylpyridine; oxalyl dichloride; 20 % Pd(OH)2/C; water; hydrogen; acetic acid; dimethyl sulfoxide;
In
dichloromethane; ethyl acetate;
DOI:10.1055/s-0030-1260586
