<4(R^*,S^*),5(S^*,R^*)-trans>-2-(trichloromethyl)-4-benzyl-5-<1-(R^*,S^*)-hydroxyethyl>-2-oxazoline

Base Information

• Chemical Name: <4(R^*,S^*),5(S^*,R^*)-trans>-2-(trichloromethyl)-4-benzyl-5-<1-(R^*,S^*)-hydroxyethyl>-2-oxazoline
• CAS No.: 110079-76-0
• Molecular Formula: C₁₃H₁₄Cl₃NO₂
• Molecular Weight: 322.619

Synonyms:<4(R^*,S^*),5(S^*,R^*)-trans>-2-(trichloromethyl)-4-benzyl-5-<1-(R^*,S^*)-hydroxyethyl>-2-oxazoline

Chemical Property of <4(R^*,S^*),5(S^*,R^*)-trans>-2-(trichloromethyl)-4-benzyl-5-<1-(R^*,S^*)-hydroxyethyl>-2-oxazoline

Chemical Property:

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Technology Process of <4(R^*,S^*),5(S^*,R^*)-trans>-2-(trichloromethyl)-4-benzyl-5-<1-(R^*,S^*)-hydroxyethyl>-2-oxazoline

There total 12 articles about <4(R^*,S^*),5(S^*,R^*)-trans>-2-(trichloromethyl)-4-benzyl-5-<1-(R^*,S^*)-hydroxyethyl>-2-oxazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N-(xylo-3,4-epoxy-1-phenylpent-2-yl)trichloroacetamide (110169-90-9) → (R)-1-((4S,5S)-4-Benzyl-2-trichloromethyl-4,5-dihydro-oxazol-5-yl)-ethanol (110079-76-0)

Guidance literature:

In methanol; for 3h; Heating; Amberlite resin;

DOI:10.1021/jo00232a014

Reference yield: 92.0%

N-(ribo-3,4-epoxy-1-phenylpent-2-yl)trichloroacetamide (110169-88-5) → <4(R*,S*),5(S*,R*)-trans>-2-(trichloromethyl)-4-benzyl-5-<1-(R*,S*)-hydroxyethyl>-2-oxazoline (110079-76-0)

Guidance literature:

With Amberlite resin; In methanol; for 3h; Heating;

DOI:10.1021/jo00232a014

Reference yield: 60.0%

N-((Z)-1-phenylpent-3-en-2-yl)trichloroacetamide (110079-69-1) → <4(R*,S*),5(S*,R*)-trans>-2-(trichloromethyl)-4-benzyl-5-<1-(R*,S*)-hydroxyethyl>-2-oxazoline (110079-76-0) + N-(arabino-3,4-epoxy-1-phenylpent-2-yl)trichloroacetamide (110079-75-9)

Guidance literature:

With tert.-butylhydroperoxide; hexacarbonyl molybdenum; In dichloromethane; benzene; at 84 ℃; for 3.5h;

DOI:10.1021/jo00232a014

upstream raw materials:

N-((Z)-1-phenylpent-3-en-2-yl)trichloroacetamide

N-(ribo-3,4-epoxy-1-phenylpent-2-yl)trichloroacetamide

1-phenylpent-3-yn-2-ol

phenylacetaldehyde

Downstream raw materials:

<4(R^*,S^*),5(R^*,S^*)-cis>-2-(trichloromethyl)-4-benzyl-5-<1(S^*,R^*)-acetoxyethyl>-2-oxazoline

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