diethyl 2,2'-disulfanediylbis(4-(4-bromophenyl)-6-methylpyrimidine-5-carboxylate)

Base Information

Chemical Name:diethyl 2,2'-disulfanediylbis(4-(4-bromophenyl)-6-methylpyrimidine-5-carboxylate)
CAS No.:1606128-31-7
Molecular Formula:C₂₈H₂₄Br₂N₄O₄S₂
Molecular Weight:704.463
Hs Code.:

Synonyms:diethyl 2,2'-disulfanediylbis(4-(4-bromophenyl)-6-methylpyrimidine-5-carboxylate)

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Chemical Property of diethyl 2,2'-disulfanediylbis(4-(4-bromophenyl)-6-methylpyrimidine-5-carboxylate)

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Technology Process of diethyl 2,2'-disulfanediylbis(4-(4-bromophenyl)-6-methylpyrimidine-5-carboxylate)

There total 1 articles about diethyl 2,2'-disulfanediylbis(4-(4-bromophenyl)-6-methylpyrimidine-5-carboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 123629-46-9
5-ethoxycarbonyl-6-methyl-4-(4-bromophenyl)-3,4-dihydropyrimidin-2(1H)-thione

: 1606128-31-7
diethyl 2,2'-disulfanediylbis(4-(4-bromophenyl)-6-methylpyrimidine-5-carboxylate)

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 6h; Cooling with ice; Inert atmosphere; Schlenk technique;
DOI:10.1002/adsc.201300776

Reference yield: 89.0%

: 1606128-31-7
diethyl 2,2'-disulfanediylbis(4-(4-bromophenyl)-6-methylpyrimidine-5-carboxylate)

: 98-80-6
phenylboronic acid

: ethyl 4-(4-bromophenyl)-6-methyl-2-phenylpyrimidine-5-carboxylate

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate; In 1,4-dioxane; at 110 ℃; for 12h; chemoselective reaction; Inert atmosphere; Sealed tube; Schlenk technique;
DOI:10.1002/adsc.201300776

Reference yield: 87.0%

: 120-72-9
indole

: 1606128-31-7
diethyl 2,2'-disulfanediylbis(4-(4-bromophenyl)-6-methylpyrimidine-5-carboxylate)

: ethyl 4-(4-bromophenyl)-2-(1H-indol-1-yl)-6-methylpyrimidine-5-carboxylate

Guidance literature:: With copper(I) thiophene-2-carboxylate; caesium carbonate; In 1,4-dioxane; at 120 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1055/s-0035-1561946