(E)-ethyl 3-[3-acetoxy-4-(neopentyloxysulfonyloxy)phenyl]acrylate

Base Information

• Chemical Name: (E)-ethyl 3-[3-acetoxy-4-(neopentyloxysulfonyloxy)phenyl]acrylate
• CAS No.: 1258842-37-3
• Molecular Formula: C₁₈H₂₄O₈S
• Molecular Weight: 400.45
• Mol file: 1258842-37-3.mol

Synonyms:(E)-ethyl 3-[3-acetoxy-4-(neopentyloxysulfonyloxy)phenyl]acrylate

Chemical Property of (E)-ethyl 3-[3-acetoxy-4-(neopentyloxysulfonyloxy)phenyl]acrylate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (E)-ethyl 3-[3-acetoxy-4-(neopentyloxysulfonyloxy)phenyl]acrylate

There total 1 articles about (E)-ethyl 3-[3-acetoxy-4-(neopentyloxysulfonyloxy)phenyl]acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

neopentyl sulfurochloridate (764-08-9) + 3-acetoxy-4-hydroxycinnamic acid ethyl ester (1258842-36-2) → (E)-ethyl 3-[3-acetoxy-4-(neopentyloxysulfonyloxy)phenyl]acrylate (1258842-37-3)

Guidance literature:

With dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1039/c0ob00137f

Reference yield:

(E)-ethyl 3-[3-acetoxy-4-(neopentyloxysulfonyloxy)phenyl]acrylate (1258842-37-3) → C13H13O8S(1-)*Na(1+)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 60 ℃; for 24h;

DOI:10.1039/c0ob00137f

upstream raw materials:

neopentyl sulfurochloridate

3-acetoxy-4-hydroxycinnamic acid ethyl ester