C₅₂H₄₃N₁₃O₈S₅

Base Information

Chemical Name:C₅₂H₄₃N₁₃O₈S₅
CAS No.:1607794-67-1
Molecular Formula:C₅₂H₄₃N₁₃O₈S₅
Molecular Weight:1138.33
Hs Code.:

C<sub>52</sub>H<sub>43</sub>N<sub>13</sub>O<sub>8</sub>S<sub>5</sub>

Synonyms:C₅₂H₄₃N₁₃O₈S₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₂H₄₃N₁₃O₈S₅

Chemical Property:

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Technology Process of C₅₂H₄₃N₁₃O₈S₅

There total 3 articles about C₅₂H₄₃N₁₃O₈S₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1607794-65-9
C₅₂H₄₂N₁₂O₉S₅

: 1607794-67-1
C₅₂H₄₃N₁₃O₈S₅

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; ammonium bicarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 28h;
DOI:10.1021/jm500062g

Reference yield:

: C₅₄H₄₈N₁₂O₁₀S₅

: 1607794-67-1
C₅₂H₄₃N₁₃O₈S₅

Guidance literature:: Multi-step reaction with 3 steps

1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 20 °C

2: lithium hydroxide / tetrahydrofuran; water / 17 h / 20 °C

3: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; ammonium bicarbonate / N,N-dimethyl-formamide / 28 h / 0 - 20 °C

With 1-hydroxy-7-aza-benzotriazole; ammonium bicarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/jm500062g

Reference yield:

: 1607794-64-8
C₅₄H₄₆N₁₂O₉S₅

: 1607794-67-1
C₅₂H₄₃N₁₃O₈S₅

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide / tetrahydrofuran; water / 17 h / 20 °C

2: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; ammonium bicarbonate / N,N-dimethyl-formamide / 28 h / 0 - 20 °C

With 1-hydroxy-7-aza-benzotriazole; ammonium bicarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/jm500062g