1,3,4-tri-O-acetyl-6-azido-2-benzyloxycarbonylamino-2,6-dideoxy-D-mannose

Base Information

Chemical Name:1,3,4-tri-O-acetyl-6-azido-2-benzyloxycarbonylamino-2,6-dideoxy-D-mannose
CAS No.:174091-48-6
Molecular Formula:C₂₀H₂₄N₄O₉
Molecular Weight:464.432
Hs Code.:

Synonyms:1,3,4-tri-O-acetyl-6-azido-2-benzyloxycarbonylamino-2,6-dideoxy-D-mannose

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Chemical Property of 1,3,4-tri-O-acetyl-6-azido-2-benzyloxycarbonylamino-2,6-dideoxy-D-mannose

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Technology Process of 1,3,4-tri-O-acetyl-6-azido-2-benzyloxycarbonylamino-2,6-dideoxy-D-mannose

There total 3 articles about 1,3,4-tri-O-acetyl-6-azido-2-benzyloxycarbonylamino-2,6-dideoxy-D-mannose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 174091-47-5
1,3,4-tri-O-acetyl-2-benzyloxycarbonylamine-2-deoxy-6-O-p-tolylsulfonyl-D-mannose

: 174091-48-6
1,3,4-tri-O-acetyl-6-azido-2-benzyloxycarbonylamino-2,6-dideoxy-D-mannose

Guidance literature:: With lithium azide; In N,N-dimethyl-formamide; at 70 - 80 ℃; for 3h;
DOI:10.1016/0008-6215(95)00295-2

Reference yield:

: 3006-58-4,7474-40-0,13030-01-8,42890-10-8,42973-23-9,77059-32-6,121785-09-9
2-<(benzyloxycarbonyl)amino>-2-deoxy-D-mannopyranose

: 174091-48-6
1,3,4-tri-O-acetyl-6-azido-2-benzyloxycarbonylamino-2,6-dideoxy-D-mannose

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / 7 h / Ambient temperature

2: pyridine / CH₂Cl₂ / 10 h / Ambient temperature

3: 54 percent / LiN₃ / dimethylformamide / 3 h / 70 - 80 °C

With pyridine; lithium azide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(95)00295-2

Reference yield:

: Toluene-4-sulfonic acid (2R,3S,4R,5S)-5-benzyloxycarbonylamino-3,4,6-trihydroxy-tetrahydro-pyran-2-ylmethyl ester

: 174091-48-6
1,3,4-tri-O-acetyl-6-azido-2-benzyloxycarbonylamino-2,6-dideoxy-D-mannose

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 10 h / Ambient temperature

2: 54 percent / LiN₃ / dimethylformamide / 3 h / 70 - 80 °C

With pyridine; lithium azide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(95)00295-2