N-(tert-butyloxycarbonyl)-D-leucyl-L-prolyl-[(4-carbamimidoyl)benzyl]amide

Base Information

Chemical Name:N-(tert-butyloxycarbonyl)-D-leucyl-L-prolyl-[(4-carbamimidoyl)benzyl]amide
CAS No.:1375059-79-2
Molecular Formula:C₂₄H₃₇N₅O₄
Molecular Weight:459.589
Hs Code.:

Synonyms:N-(tert-butyloxycarbonyl)-D-leucyl-L-prolyl-[(4-carbamimidoyl)benzyl]amide

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Chemical Property of N-(tert-butyloxycarbonyl)-D-leucyl-L-prolyl-[(4-carbamimidoyl)benzyl]amide

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Technology Process of N-(tert-butyloxycarbonyl)-D-leucyl-L-prolyl-[(4-carbamimidoyl)benzyl]amide

There total 9 articles about N-(tert-butyloxycarbonyl)-D-leucyl-L-prolyl-[(4-carbamimidoyl)benzyl]amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₇N₅O₅

: 1375059-79-2
N-(tert-butyloxycarbonyl)-D-leucyl-L-prolyl-[(4-carbamimidoyl)benzyl]amide

Guidance literature:: C₂₄H₃₇N₅O₅; With acetic anhydride; In acetic acid; for 0.5h;

With palladium 10% on activated carbon; hydrogen; In acetic acid; for 12h;

With hydrogenchloride; In methanol; acetic acid; at 0 ℃; for 3h;
DOI:10.1016/j.ejmech.2015.03.059

Reference yield:

: 1215172-80-7
C₃₂H₄₃N₅O₆

: 1375059-79-2
N-(tert-butyloxycarbonyl)-D-leucyl-L-prolyl-[(4-carbamimidoyl)benzyl]amide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; for 48h;
DOI:10.1021/jm9016416

Reference yield:

: tert-butyl ((R)-1-((2S)-2-((4-cyanobenzyl)carbamoyl)pyrrolidin-1-yl)-4-methyl-1-oxopetan-2-yl)carbamate

: 1375059-79-2
N-(tert-butyloxycarbonyl)-D-leucyl-L-prolyl-[(4-carbamimidoyl)benzyl]amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine; hydroxylamine hydrochloride / methanol / 16 h

2.1: acetic anhydride / acetic acid / 0.5 h

2.2: 12 h

2.3: 3 h / 0 °C

With hydroxylamine hydrochloride; acetic anhydride; N-ethyl-N,N-diisopropylamine; In methanol; acetic acid;
DOI:10.1016/j.ejmech.2015.03.059