N-[(2R,3R,4R,5S,6R)-2-((2R,3R,4R,5S,6S)-3-Allyloxy-5-benzyloxy-2-methoxy-6-methyl-tetrahydro-pyran-4-yloxy)-4-benzyloxy-5-hydroxy-6-methyl-tetrahydro-pyran-3-yl]-acetamide

Base Information

Chemical Name:N-[(2R,3R,4R,5S,6R)-2-((2R,3R,4R,5S,6S)-3-Allyloxy-5-benzyloxy-2-methoxy-6-methyl-tetrahydro-pyran-4-yloxy)-4-benzyloxy-5-hydroxy-6-methyl-tetrahydro-pyran-3-yl]-acetamide
CAS No.:902768-09-6
Molecular Formula:C₃₂H₄₃NO₉
Molecular Weight:585.695
Hs Code.:

N-[(2R,3R,4R,5S,6R)-2-((2R,3R,4R,5S,6S)-3-Allyloxy-5-benzyloxy-2-methoxy-6-methyl-tetrahydro-pyran-4-yloxy)-4-benzyloxy-5-hydroxy-6-methyl-tetrahydro-pyran-3-yl]-acetamide

Synonyms:N-[(2R,3R,4R,5S,6R)-2-((2R,3R,4R,5S,6S)-3-Allyloxy-5-benzyloxy-2-methoxy-6-methyl-tetrahydro-pyran-4-yloxy)-4-benzyloxy-5-hydroxy-6-methyl-tetrahydro-pyran-3-yl]-acetamide

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Chemical Property of N-[(2R,3R,4R,5S,6R)-2-((2R,3R,4R,5S,6S)-3-Allyloxy-5-benzyloxy-2-methoxy-6-methyl-tetrahydro-pyran-4-yloxy)-4-benzyloxy-5-hydroxy-6-methyl-tetrahydro-pyran-3-yl]-acetamide

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Technology Process of N-[(2R,3R,4R,5S,6R)-2-((2R,3R,4R,5S,6S)-3-Allyloxy-5-benzyloxy-2-methoxy-6-methyl-tetrahydro-pyran-4-yloxy)-4-benzyloxy-5-hydroxy-6-methyl-tetrahydro-pyran-3-yl]-acetamide

There total 11 articles about N-[(2R,3R,4R,5S,6R)-2-((2R,3R,4R,5S,6S)-3-Allyloxy-5-benzyloxy-2-methoxy-6-methyl-tetrahydro-pyran-4-yloxy)-4-benzyloxy-5-hydroxy-6-methyl-tetrahydro-pyran-3-yl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Acetic acid (2R,3S,4R,5R,6R)-5-acetylamino-6-((2R,3R,4R,5S,6S)-3-allyloxy-5-benzyloxy-2-methoxy-6-methyl-tetrahydro-pyran-4-yloxy)-4-benzyloxy-2-methyl-tetrahydro-pyran-3-yl ester

: 902768-09-6
N-[(2R,3R,4R,5S,6R)-2-((2R,3R,4R,5S,6S)-3-Allyloxy-5-benzyloxy-2-methoxy-6-methyl-tetrahydro-pyran-4-yloxy)-4-benzyloxy-5-hydroxy-6-methyl-tetrahydro-pyran-3-yl]-acetamide

Guidance literature:: With sodium methylate; In methanol; dichloromethane; at 20 ℃; for 4h;
DOI:10.1055/s-2006-939057

Reference yield:

: phenyl 2-azido-2-deoxy-1-seleno-α-D-fucopyranoside

: 902768-09-6
N-[(2R,3R,4R,5S,6R)-2-((2R,3R,4R,5S,6S)-3-Allyloxy-5-benzyloxy-2-methoxy-6-methyl-tetrahydro-pyran-4-yloxy)-4-benzyloxy-5-hydroxy-6-methyl-tetrahydro-pyran-3-yl]-acetamide

Guidance literature:: Multi-step reaction with 8 steps

1.1: Bu₂SnO / benzene; methanol / 1.5 h / Heating

1.2: TBAB / toluene / 3 h / 65 °C

2.1: pyridine / 20 °C

3.1: NIS; water / tetrahydrofuran / 1 h / 20 °C

4.1: NaH / CH₂Cl₂ / 2 h / 0 °C

5.1: 89 percent / TMSOTf / CH₂Cl₂ / 3 h / 0 °C

6.1: PPh₃; water / tetrahydrofuran / 20 °C

7.1: pyridine / 20 °C

8.1: NaOMe / methanol; CH₂Cl₂ / 4 h / 20 °C

With pyridine; N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; water; sodium methylate; sodium hydride; di(n-butyl)tin oxide; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; benzene; 6.1: Staudinger reaction;
DOI:10.1055/s-2006-939057

Reference yield:

: Acetic acid (2R,3S,4R,5R)-5-azido-4-benzyloxy-6-hydroxy-2-methyl-tetrahydro-pyran-3-yl ester

: 902768-09-6
N-[(2R,3R,4R,5S,6R)-2-((2R,3R,4R,5S,6S)-3-Allyloxy-5-benzyloxy-2-methoxy-6-methyl-tetrahydro-pyran-4-yloxy)-4-benzyloxy-5-hydroxy-6-methyl-tetrahydro-pyran-3-yl]-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: NaH / CH₂Cl₂ / 2 h / 0 °C

2: 89 percent / TMSOTf / CH₂Cl₂ / 3 h / 0 °C

3: PPh₃; water / tetrahydrofuran / 20 °C

4: pyridine / 20 °C

5: NaOMe / methanol; CH₂Cl₂ / 4 h / 20 °C

With pyridine; trimethylsilyl trifluoromethanesulfonate; water; sodium methylate; sodium hydride; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; 3: Staudinger reaction;
DOI:10.1055/s-2006-939057