N⁹-benzyl-N¹,N¹⁷-diformyl-N⁵,N¹³-ditosyl-5,9,13-triaza-1,17-heptadecanediamine

Base Information

Chemical Name:N⁹-benzyl-N¹,N¹⁷-diformyl-N⁵,N¹³-ditosyl-5,9,13-triaza-1,17-heptadecanediamine
CAS No.:164913-00-2
Molecular Formula:C₃₇H₅₃N₅O₆S₂
Molecular Weight:727.99
Hs Code.:

N<sup>9</sup>-benzyl-N<sup>1</sup>,N<sup>17</sup>-diformyl-N<sup>5</sup>,N<sup>13</sup>-ditosyl-5,9,13-triaza-1,17-heptadecanediamine

Synonyms:N⁹-benzyl-N¹,N¹⁷-diformyl-N⁵,N¹³-ditosyl-5,9,13-triaza-1,17-heptadecanediamine

Suppliers and Price of N⁹-benzyl-N¹,N¹⁷-diformyl-N⁵,N¹³-ditosyl-5,9,13-triaza-1,17-heptadecanediamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N⁹-benzyl-N¹,N¹⁷-diformyl-N⁵,N¹³-ditosyl-5,9,13-triaza-1,17-heptadecanediamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N⁹-benzyl-N¹,N¹⁷-diformyl-N⁵,N¹³-ditosyl-5,9,13-triaza-1,17-heptadecanediamine

There total 5 articles about N⁹-benzyl-N¹,N¹⁷-diformyl-N⁵,N¹³-ditosyl-5,9,13-triaza-1,17-heptadecanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 164912-97-4
N⁹-benzyl-1,17-diphthalimido-N⁵,N¹³-ditosyl-5,9,13-triazaheptadecane

: 164913-00-2
N⁹-benzyl-N¹,N¹⁷-diformyl-N⁵,N¹³-ditosyl-5,9,13-triaza-1,17-heptadecanediamine

Guidance literature:: With hydrazine hydrate; at 75 ℃; for 48h;
DOI:10.1246/bcsj.73.693

Reference yield:

: 5394-18-3
2-(4-bromobutyl)isoindoline-1,3-dione

: 164913-00-2
N⁹-benzyl-N¹,N¹⁷-diformyl-N⁵,N¹³-ditosyl-5,9,13-triaza-1,17-heptadecanediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / potassium carbonate / dimethylformamide / 96 h / 20 °C

2: 90 percent / hydrazine hydrate / 48 h / 75 °C

With potassium carbonate; hydrazine hydrate; In N,N-dimethyl-formamide; 1: Alkylation / 2: Formylation;
DOI:10.1246/bcsj.73.693

Reference yield:

: 3245-95-2
N-(3-bromo-propyl)-4-methyl-benzenesulfonamide

: 164913-00-2
N⁹-benzyl-N¹,N¹⁷-diformyl-N⁵,N¹³-ditosyl-5,9,13-triaza-1,17-heptadecanediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / sodium hydrogen carbonate / acetonitrile / 70 h / 70 °C

2: 99 percent / potassium carbonate / dimethylformamide / 96 h / 20 °C

3: 90 percent / hydrazine hydrate / 48 h / 75 °C

With sodium hydrogencarbonate; potassium carbonate; hydrazine hydrate; In N,N-dimethyl-formamide; acetonitrile; 1: Alkylation / 2: Alkylation / 3: Formylation;
DOI:10.1246/bcsj.73.693