Technology Process of N,N-di-(4-aminophenyl)-1-aminopyrene
There total 4 articles about N,N-di-(4-aminophenyl)-1-aminopyrene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrazine hydrate;
In
ethanol;
for 16h;
Inert atmosphere;
Reflux;
DOI:10.1039/c0jm00495b
- Guidance literature:
-
Multi-step reaction with 4 steps
1: copper(II) nitrate trihydrate; acetic anhydride / ethyl acetate / 24 h / 55 °C / Inert atmosphere
2: palladium 10% on activated carbon; hydrazine hydrate / tetrahydrofuran; ethanol / 12 h / Inert atmosphere; Reflux
3: cesium fluoride / dimethyl sulfoxide / 18 h / 140 °C / Inert atmosphere
4: palladium 10% on activated carbon; hydrazine hydrate / ethanol / 16 h / Inert atmosphere; Reflux
With
copper(II) nitrate trihydrate; palladium 10% on activated carbon; acetic anhydride; hydrazine hydrate; cesium fluoride;
In
tetrahydrofuran; ethanol; dimethyl sulfoxide; ethyl acetate;
DOI:10.1039/c0jm00495b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium 10% on activated carbon; hydrazine hydrate / tetrahydrofuran; ethanol / 12 h / Inert atmosphere; Reflux
2: cesium fluoride / dimethyl sulfoxide / 18 h / 140 °C / Inert atmosphere
3: palladium 10% on activated carbon; hydrazine hydrate / ethanol / 16 h / Inert atmosphere; Reflux
With
palladium 10% on activated carbon; hydrazine hydrate; cesium fluoride;
In
tetrahydrofuran; ethanol; dimethyl sulfoxide;
DOI:10.1039/c0jm00495b
