dimethyl 2-(p-nitrocinnamyl)-2-propargylmalonate

Base Information

Chemical Name:dimethyl 2-(p-nitrocinnamyl)-2-propargylmalonate
CAS No.:884492-30-2
Molecular Formula:C₁₇H₁₇NO₆
Molecular Weight:331.325
Hs Code.:

Synonyms:dimethyl 2-(p-nitrocinnamyl)-2-propargylmalonate

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Chemical Property of dimethyl 2-(p-nitrocinnamyl)-2-propargylmalonate

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Technology Process of dimethyl 2-(p-nitrocinnamyl)-2-propargylmalonate

There total 1 articles about dimethyl 2-(p-nitrocinnamyl)-2-propargylmalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 79750-53-1
(E)-3-(4-nitrophenyl)prop-2-en-1-yl bromide

: 95124-07-5
dimethyl (prop-2-yn-1-yl)malonate

: 884492-30-2
dimethyl 2-(p-nitrocinnamyl)-2-propargylmalonate

Guidance literature:: dimethyl (prop-2-yn-1-yl)malonate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h;

(E)-3-(4-nitrophenyl)prop-2-en-1-yl bromide; In N,N-dimethyl-formamide; at 23 ℃; for 16h;
DOI:10.1002/chem.200501088

Reference yield:

: 884492-30-2
dimethyl 2-(p-nitrocinnamyl)-2-propargylmalonate

: 2-[3-(4-nitro-phenyl)-propenyl]-2-prop-2-ynyl-malonic acid dimethyl ester

: dimethyl 2-((E)-3-(4-nitrophenyl)allyl)-2-(2-oxopropyl)malonate

: 2-[3-(4-nitro-phenyl)-propenyl]-2-(2-oxo-propyl)-malonic acid dimethyl ester

Guidance literature:: With water; [Ph₃P-Au-(NCCH₃)]⁽¹⁺⁾*SbF₆^(1-); In methanol; at 23 ℃; for 72h;
DOI:10.1002/chem.200501088

Reference yield:

: 884492-30-2
dimethyl 2-(p-nitrocinnamyl)-2-propargylmalonate

: dimethyl 5-((Z)-4-nitrobenzylidene)cyclohex-3-ene-1,1-dicarboxylate

: (E)-1,1-dimethyl 3-(4-nitrostyryl)cyclopent-3-ene-1,1-dicarboxylate

Guidance literature:: With silver hexafluoroantimonate; chlorotriphenylphosphinegold(I); In dichloromethane; at 23 ℃; for 3h; Further Variations:; Catalysts; time; Product distribution;
DOI:10.1002/chem.200501088