N-(2-ethylhexyl)-1,7-(3’,5’-di-t-butylphenoxy)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide

Base Information

• Chemical Name: N-(2-ethylhexyl)-1,7-(3’,5’-di-t-butylphenoxy)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide
• CAS No.: 457892-77-2
• Molecular Formula: C₆₀H₆₅NO₇
• Molecular Weight: 912.179

Synonyms:N-(2-ethylhexyl)-1,7-(3’,5’-di-t-butylphenoxy)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide

Chemical Property of N-(2-ethylhexyl)-1,7-(3’,5’-di-t-butylphenoxy)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide

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Technology Process of N-(2-ethylhexyl)-1,7-(3’,5’-di-t-butylphenoxy)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide

There total 4 articles about N-(2-ethylhexyl)-1,7-(3’,5’-di-t-butylphenoxy)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

2-Ethylhexylamine (104-75-6) + 1,7-(3’,5‘-di-t-butylphenoxy)perylene-3,4:9,10-tetracarboxydianhydride (404871-21-2) → N-(2-ethylhexyl)-1,7-(3’,5’-di-t-butylphenoxy)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide (457892-77-2)

Guidance literature:

With 1H-imidazole; trifluoroacetic acid; In chloroform; for 72h; Heating;

DOI:10.1021/ja026286k

Reference yield: 24.0%

2-Ethylhexylamine (104-75-6) → N-(2-ethylhexyl)-1,7-(3’,5’-di-t-butylphenoxy)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide (457892-77-2)

Guidance literature:

1,7-(3’,5‘-di-t-butylphenoxy)perylene-3,4:9,10-tetracarboxydianhydride; With 1H-imidazole; In chloroform; for 1h; Heating / reflux;

2-Ethylhexylamine; With trifluoroacetic acid; In chloroform; for 73h; Heating / reflux;

Reference yield:

2-Ethylhexylamine (104-75-6) + 1,7-(3’,5‘-di-t-butylphenoxy)perylene-3,4:9,10-tetracarboxydianhydride (404871-21-2) → N-(2-ethylhexyl)-1,7-(3’,5’-di-t-butylphenoxy)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide (457892-77-2) + 5,12-bis-(3,5-di-tert-butyl-phenoxy)-2,9-bis-(2-ethyl-hexyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone (876301-65-4)

Guidance literature:

With pyridine; for 2h; Heating;

DOI:10.1021/ja0398215

upstream raw materials:

2-Ethylhexylamine

1,7-(3’,5‘-di-t-butylphenoxy)perylene-3,4:9,10-tetracarboxydianhydride

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

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