C₂₆H₂₇N₃OS

Base Information

Chemical Name:C₂₆H₂₇N₃OS
CAS No.:1340580-89-3
Molecular Formula:C₂₆H₂₇N₃OS
Molecular Weight:429.586
Hs Code.:

C<sub>26</sub>H<sub>27</sub>N<sub>3</sub>OS

Synonyms:C₂₆H₂₇N₃OS

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Chemical Property of C₂₆H₂₇N₃OS

Chemical Property:

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Technology Process of C₂₆H₂₇N₃OS

There total 9 articles about C₂₆H₂₇N₃OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: tert-butyl benzyl(3-(6-(thiazole-2-carbonyl)-3,4-dihydro-1H-carbazol-9(2H)-yl)propyl)carbamate

: 1340580-89-3
C₂₆H₂₇N₃OS

Guidance literature:: With hydrogenchloride; In ethyl acetate;
DOI:10.1039/c2md20211e

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1340580-89-3
C₂₆H₂₇N₃OS

Guidance literature:: Multi-step reaction with 9 steps

1.1: N-Bromosuccinimide; ammonium acetate / diethyl ether / 0.5 h / 20 °C

2.1: 2-methoxy-ethanol / 12 h / 130 °C / Inert atmosphere

3.1: potassium hydroxide / dimethyl sulfoxide / 3 h / 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

5.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C

6.1: lithium hydroxide / tetrahydrofuran; methanol; water / 24 h / 50 °C

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 12 h / 20 °C

8.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

8.2: 0.5 h / Inert atmosphere

9.1: hydrogenchloride / ethyl acetate

With hydrogenchloride; dmap; N-Bromosuccinimide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; ammonium acetate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; 2-methoxy-ethanol; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/c2md20211e

Reference yield:

: 21660-16-2
1,2,3,4-tetrahydrocarbazole-6-carboxylic acid ethyl ester

: 1340580-89-3
C₂₆H₂₇N₃OS

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 3 h / 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

3.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C

4.1: lithium hydroxide / tetrahydrofuran; methanol; water / 24 h / 50 °C

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 12 h / 20 °C

6.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

6.2: 0.5 h / Inert atmosphere

7.1: hydrogenchloride / ethyl acetate

With hydrogenchloride; dmap; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/c2md20211e