6-O-benzyl-2-azido-3-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-α-D-glucopyranosyl-(1->4)-methyl 3-O-benzyl-1,2-O-isopropylidene-β-L-idopyranosuronate

Base Information

Chemical Name:6-O-benzyl-2-azido-3-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-α-D-glucopyranosyl-(1->4)-methyl 3-O-benzyl-1,2-O-isopropylidene-β-L-idopyranosuronate
CAS No.:1190921-24-4
Molecular Formula:C₄₅H₅₁N₃O₁₂
Molecular Weight:825.913
Hs Code.:

Synonyms:6-O-benzyl-2-azido-3-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-α-D-glucopyranosyl-(1->4)-methyl 3-O-benzyl-1,2-O-isopropylidene-β-L-idopyranosuronate

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Chemical Property of 6-O-benzyl-2-azido-3-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-α-D-glucopyranosyl-(1->4)-methyl 3-O-benzyl-1,2-O-isopropylidene-β-L-idopyranosuronate

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Technology Process of 6-O-benzyl-2-azido-3-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-α-D-glucopyranosyl-(1->4)-methyl 3-O-benzyl-1,2-O-isopropylidene-β-L-idopyranosuronate

There total 1 articles about 6-O-benzyl-2-azido-3-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-α-D-glucopyranosyl-(1->4)-methyl 3-O-benzyl-1,2-O-isopropylidene-β-L-idopyranosuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: phenyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-1-thio-β-D-glucopyranoside

: 444118-44-9
1,2-O-isopropylidene-3-O-benzyl-4-O-trichloroacetyl-6-methyl-α-L-idonic acid

: 1190921-24-4
6-O-benzyl-2-azido-3-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-α-D-glucopyranosyl-(1->4)-methyl 3-O-benzyl-1,2-O-isopropylidene-β-L-idopyranosuronate

Guidance literature:: phenyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-1-thio-β-D-glucopyranoside; 1,2-O-isopropylidene-3-O-benzyl-4-O-trichloroacetyl-6-methyl-α-L-idonic acid; In dichloromethane; at 0 ℃; Molecular sieve; Inert atmosphere;

With N-iodo-succinimide; In dichloromethane;

With silver trifluoromethanesulfonate; In dichloromethane; stereoselective reaction;
DOI:10.1021/ol901723m