C₄₄H₇₅Si₃O₅N

Base Information

Chemical Name:C₄₄H₇₅Si₃O₅N
CAS No.:930807-81-1
Molecular Formula:C₄₄H₇₅NO₅Si₃
Molecular Weight:782.34
Hs Code.:

C<sub>44</sub>H<sub>75</sub>Si<sub>3</sub>O<sub>5</sub>N

Synonyms:C₄₄H₇₅Si₃O₅N

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Chemical Property of C₄₄H₇₅Si₃O₅N

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Technology Process of C₄₄H₇₅Si₃O₅N

There total 8 articles about C₄₄H₇₅Si₃O₅N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 930807-80-0
C₄₄H₇₃Si₃O₅N₃

: 930807-81-1
C₄₄H₇₅Si₃O₅N

Guidance literature:: With water; triphenylphosphine; In tetrahydrofuran; for 20h; Heating;
DOI:10.1002/anie.200603656

Reference yield:

: 930807-74-2
C₃₄H₅₀O₇Si

: 930807-81-1
C₄₄H₇₅Si₃O₅N

Guidance literature:: Multi-step reaction with 7 steps

1: 93 percent / 2,6-lutidine / CH₂Cl₂ / 1.25 h / -78 °C

2: 94 percent / Dess-Martin periodinane / CH₂Cl₂ / 2 h / 20 °C

3: 77 percent / ethyl pivalate / tetrahydrofuran; toluene / 15 h / 80 °C

4: 93 percent / p-toluenesulfonic acid / methanol / 1.5 h / 40 °C

5: 76 percent / imidazole / CH₂Cl₂ / 0.5 h / -78 °C

6: 88 percent / triphenylphosphine; diphenylphosphorylazide; diethylazodicarboxylate / tetrahydrofuran; toluene / 2 h / 20 °C

7: 74 percent / triphenylphosphine; water / tetrahydrofuran / 20 h / Heating

With 1H-imidazole; 2,6-dimethylpyridine; 2,2-dimethyl-propanoic acid ethyl ester; diphenylphosphoranyl azide; water; Dess-Martin periodane; toluene-4-sulfonic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; toluene; 2: Dess-Martin oxidation / 6: Mitsunobu reaction / 7: Staudinger reduction;
DOI:10.1002/anie.200603656

Reference yield:

: 930807-79-7
C₄₄H₇₄Si₃O₆

: 930807-81-1
C₄₄H₇₅Si₃O₅N

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / triphenylphosphine; diphenylphosphorylazide; diethylazodicarboxylate / tetrahydrofuran; toluene / 2 h / 20 °C

2: 74 percent / triphenylphosphine; water / tetrahydrofuran / 20 h / Heating

With diphenylphosphoranyl azide; water; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; 1: Mitsunobu reaction / 2: Staudinger reduction;
DOI:10.1002/anie.200603656