dimethyl N-<4-(2,4-dioxo-1,2,3,4-tetrahydro-3-quinazolinylphenylsulphonyl)>dithiocarbonoimidate

Base Information

Chemical Name:dimethyl N-<4-(2,4-dioxo-1,2,3,4-tetrahydro-3-quinazolinylphenylsulphonyl)>dithiocarbonoimidate
CAS No.:170806-08-3
Molecular Formula:C₁₇H₁₅N₃O₄S₃
Molecular Weight:421.522
Hs Code.:

Synonyms:dimethyl N-<4-(2,4-dioxo-1,2,3,4-tetrahydro-3-quinazolinylphenylsulphonyl)>dithiocarbonoimidate

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Chemical Property of dimethyl N-<4-(2,4-dioxo-1,2,3,4-tetrahydro-3-quinazolinylphenylsulphonyl)>dithiocarbonoimidate

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Technology Process of dimethyl N-<4-(2,4-dioxo-1,2,3,4-tetrahydro-3-quinazolinylphenylsulphonyl)>dithiocarbonoimidate

There total 3 articles about dimethyl N-<4-(2,4-dioxo-1,2,3,4-tetrahydro-3-quinazolinylphenylsulphonyl)>dithiocarbonoimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 170806-09-4
dimethyl N-<4-(4-oxo-2-ethylthio-3,4-dihydro-3-quinazolinylphenylsulphonyl)>dithiocarbonoimidate

: 170806-08-3
dimethyl N-<4-(2,4-dioxo-1,2,3,4-tetrahydro-3-quinazolinylphenylsulphonyl)>dithiocarbonoimidate

Guidance literature:: With hydrogenchloride; In ethanol; for 6h; Heating;

Reference yield: 31.0%

: 37960-65-9
potassium anthranilate

: 135198-17-3
dimethyl N-(4-thiomethylthiocarbonylaminophenylsulphonyl)dithiocarbonoiomidate

: 170806-08-3
dimethyl N-<4-(2,4-dioxo-1,2,3,4-tetrahydro-3-quinazolinylphenylsulphonyl)>dithiocarbonoimidate

Guidance literature:: With mercury(II) oxide; In N,N-dimethyl-formamide; at 70 ℃; for 22h;

Reference yield:

: 170806-07-2
dimethyl N-<4-(4-oxo-2-thioxo-1,2,3,4-tetrahydro-3-quinazolinylphenylsulphonyl)>dithiocarbonoimidate

: 170806-08-3
dimethyl N-<4-(2,4-dioxo-1,2,3,4-tetrahydro-3-quinazolinylphenylsulphonyl)>dithiocarbonoimidate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 5N aq. NaOH / 1.) DMF, RT, 1 h, 2.) DMF, 2 h

2: 92 percent / 6N aq. HCl / ethanol / 6 h / Heating

With hydrogenchloride; sodium hydroxide; In ethanol;