methyl 2-S-benzyl-3-benzylsulfonamido-3-deoxy-2-thio-α-D-altropyranoside

Base Information

Chemical Name:methyl 2-S-benzyl-3-benzylsulfonamido-3-deoxy-2-thio-α-D-altropyranoside
CAS No.:87236-51-9
Molecular Formula:C₂₁H₂₇NO₆S₂
Molecular Weight:453.58
Hs Code.:

Synonyms:methyl 2-S-benzyl-3-benzylsulfonamido-3-deoxy-2-thio-α-D-altropyranoside

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Chemical Property of methyl 2-S-benzyl-3-benzylsulfonamido-3-deoxy-2-thio-α-D-altropyranoside

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Technology Process of methyl 2-S-benzyl-3-benzylsulfonamido-3-deoxy-2-thio-α-D-altropyranoside

There total 6 articles about methyl 2-S-benzyl-3-benzylsulfonamido-3-deoxy-2-thio-α-D-altropyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.2%

: 87236-49-5
methyl 2-S-benzyl-4,6-O-benzylidene-3-benzylsulfonamido-3-deoxy-2-thio-α-D-altropyranoside

: 87236-50-8
1,6-anhydro-2-S-benzyl-3-benzylsulfonamido-3-deoxy-2-thio-β-D-altropyranose

: 87236-51-9
methyl 2-S-benzyl-3-benzylsulfonamido-3-deoxy-2-thio-α-D-altropyranoside

Guidance literature:: With Amberlite CG-120; In methanol; water; at 55 ℃; for 30h;
DOI:10.1016/0008-6215(83)84066-X

Reference yield:

: 10396-60-8
methyl 3-amino-4,6-O-benzylidene-3-deoxy-α-D-altropyranoside

: 87236-51-9
methyl 2-S-benzyl-3-benzylsulfonamido-3-deoxy-2-thio-α-D-altropyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / pyridine / 24 h / 0 °C

2: sodium hydroxyde 5M / 0.25 h / boiling water bath

3: 91 percent / sodium / methanol / 2 h / Heating

4: 60.2 percent / Amberlite CG-120 / methanol; H₂O / 30 h / 55 °C

With pyridine; sodium hydroxide; Amberlite CG-120; sodium; In methanol; water;
DOI:10.1016/0008-6215(83)84066-X

Reference yield:

: 87236-52-0
methyl 2,3-(N-benzylsulfonylepimino)-2,3-dideoxy-α-D-allopyranoside

: 87236-51-9
methyl 2-S-benzyl-3-benzylsulfonamido-3-deoxy-2-thio-α-D-altropyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / zinc chloride / 24 h / Ambient temperature

2: 91 percent / sodium / methanol / 2 h / Heating

3: 60.2 percent / Amberlite CG-120 / methanol; H₂O / 30 h / 55 °C

With Amberlite CG-120; sodium; zinc(II) chloride; In methanol; water;
DOI:10.1016/0008-6215(83)84066-X