N-(fluorenyl-9-methoxycarbonyl)-O-(3,4,6-tri-O-benzyl-2-tert-butoxycarbonylamino-2-deoxy-α-D-galactopyranosyl)-L-serine

Base Information

Chemical Name:N-(fluorenyl-9-methoxycarbonyl)-O-(3,4,6-tri-O-benzyl-2-tert-butoxycarbonylamino-2-deoxy-α-D-galactopyranosyl)-L-serine
CAS No.:552888-52-5
Molecular Formula:C₅₀H₅₄N₂O₁₁
Molecular Weight:858.986
Hs Code.:

Synonyms:N-(fluorenyl-9-methoxycarbonyl)-O-(3,4,6-tri-O-benzyl-2-tert-butoxycarbonylamino-2-deoxy-α-D-galactopyranosyl)-L-serine

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Chemical Property of N-(fluorenyl-9-methoxycarbonyl)-O-(3,4,6-tri-O-benzyl-2-tert-butoxycarbonylamino-2-deoxy-α-D-galactopyranosyl)-L-serine

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Technology Process of N-(fluorenyl-9-methoxycarbonyl)-O-(3,4,6-tri-O-benzyl-2-tert-butoxycarbonylamino-2-deoxy-α-D-galactopyranosyl)-L-serine

There total 3 articles about N-(fluorenyl-9-methoxycarbonyl)-O-(3,4,6-tri-O-benzyl-2-tert-butoxycarbonylamino-2-deoxy-α-D-galactopyranosyl)-L-serine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 58632-95-4
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

: 552888-51-4
O-(2-amino-3,4,6-tri-O-benzyl-2-deoxy-α-D-galactopyranosyl)-N-(fluorenyl-9-methoxycarbonyl)-L-serine

: 552888-52-5
N-(fluorenyl-9-methoxycarbonyl)-O-(3,4,6-tri-O-benzyl-2-tert-butoxycarbonylamino-2-deoxy-α-D-galactopyranosyl)-L-serine

Guidance literature:: With triethylamine; In 1,4-dioxane; water; at 20 ℃; for 3h;
DOI:10.1002/ejoc.200390142

Reference yield:

: 225663-02-5
O-(3,4,6-tri-O-benzyl-2-deoxy-2-nitro-α-D-galactopyranosyl)-N-(fluorenylmethoxycarbonyl)-L-serine tert-butyl ester

: 552888-52-5
N-(fluorenyl-9-methoxycarbonyl)-O-(3,4,6-tri-O-benzyl-2-tert-butoxycarbonylamino-2-deoxy-α-D-galactopyranosyl)-L-serine

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / Raney-Ni T₄/Pt; H₂ / ethanol / 48 h / 20 °C

2: 96 percent / trifluoroacetic acid; CH₂Cl₂ / 6 h / 20 °C

3: 84 percent / Et₃N / H₂O; dioxane / 3 h / 20 °C

With Raney-Ni T₄/Pt; hydrogen; triethylamine; In 1,4-dioxane; ethanol; dichloromethane; water; trifluoroacetic acid;
DOI:10.1002/ejoc.200390142

Reference yield:

: 552888-49-0
O-(2-amino-3,4,6-tri-O-benzyl-2-deoxy-α-D-galactopyranosyl)-N-(fluorenyl-9-methoxycarbonyl)-L-serine tert-butyl ester

: 552888-52-5
N-(fluorenyl-9-methoxycarbonyl)-O-(3,4,6-tri-O-benzyl-2-tert-butoxycarbonylamino-2-deoxy-α-D-galactopyranosyl)-L-serine

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / trifluoroacetic acid; CH₂Cl₂ / 6 h / 20 °C

2: 84 percent / Et₃N / H₂O; dioxane / 3 h / 20 °C

With triethylamine; In 1,4-dioxane; dichloromethane; water; trifluoroacetic acid;
DOI:10.1002/ejoc.200390142