C₁₂H₁₀BrNO₄S₂

Base Information

Chemical Name:C₁₂H₁₀BrNO₄S₂
CAS No.:1428510-54-6
Molecular Formula:C₁₂H₁₀BrNO₄S₂
Molecular Weight:376.252
Hs Code.:

C<sub>12</sub>H<sub>10</sub>BrNO<sub>4</sub>S<sub>2</sub>

Synonyms:C₁₂H₁₀BrNO₄S₂

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Chemical Property of C₁₂H₁₀BrNO₄S₂

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Technology Process of C₁₂H₁₀BrNO₄S₂

There total 1 articles about C₁₂H₁₀BrNO₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1375472-72-2
C₁₂H₈BrClO₄S₂

: 1428510-54-6
C₁₂H₁₀BrNO₄S₂

Guidance literature:: With ammonia; In 1,4-dioxane; at 20 ℃;
DOI:10.1016/j.bmcl.2013.01.120

Reference yield: 77.0%

: 1428510-54-6
C₁₂H₁₀BrNO₄S₂

: 1428510-55-7
C₁₁H₁₀BrNO₃S₂

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/j.bmcl.2013.01.120

Reference yield:

: 1428510-54-6
C₁₂H₁₀BrNO₄S₂

: 1170195-46-6
C₁₉H₁₉N₃O₄S₂

Guidance literature:: Multi-step reaction with 6 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

2: triphenylphosphine; carbon tetrabromide / tetrahydrofuran; dichloromethane / 20 °C

3: sodium hydride / N,N-dimethyl-formamide / 55 °C

4: sodium hydride / N,N-dimethyl-formamide / 60 °C

5: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tris-(o-tolyl)phosphine; potassium phosphate / 140 °C / Microwave irradiation

6: sodium hydroxide / water; methanol / 20 °C

With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium aluminium tetrahydride; carbon tetrabromide; sodium hydride; triphenylphosphine; tris-(o-tolyl)phosphine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 5: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.bmcl.2013.01.120