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C38H41N5O7S

Base Information
  • Chemical Name:C38H41N5O7S
  • CAS No.:1275620-50-2
  • Molecular Formula:C38H41N5O7S
  • Molecular Weight:711.839
  • Hs Code.:
C<sub>38</sub>H<sub>41</sub>N<sub>5</sub>O<sub>7</sub>S

Synonyms:C38H41N5O7S

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Chemical Property of C38H41N5O7S
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Technology Process of C38H41N5O7S

There total 14 articles about C38H41N5O7S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 ℃; for 4h;
Guidance literature:
Multi-step reaction with 13 steps
1.1: ethanol; water / 5 - 10 °C
2.1: Warmed water bath
3.1: bromine / chloroform
4.1: potassium acetate / acetone
5.1: acetic acid; phosphoric acid / 5 h / Reflux
6.1: trichlorophosphate / 2 h / Reflux
7.1: sodium t-butanolate / dimethyl sulfoxide / 1 h / 0 - 20 °C
7.2: 4 h / 10 °C
7.3: pH 6 - 7
8.1: thionyl chloride / 1 h / Reflux
9.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 20 °C
10.1: lithium hydroxide / tetrahydrofuran / 20 °C
10.2: pH < 7
11.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 20 °C
12.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 24 h / 40 °C / Inert atmosphere
13.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 4 h / 20 °C
With 4-methyl-morpholine; hydrogenchloride; thionyl chloride; phosphoric acid; bromine; potassium acetate; benzotriazol-1-ol; acetic acid; HATU; lithium hydroxide; sodium t-butanolate; trichlorophosphate; Hoveyda-Grubbs catalyst second generation; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; chloroform; water; dimethyl sulfoxide; acetone;
Guidance literature:
Multi-step reaction with 5 steps
1.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 20 °C
2.1: lithium hydroxide / tetrahydrofuran / 20 °C
2.2: pH < 7
3.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 20 °C
4.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 24 h / 40 °C / Inert atmosphere
5.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 4 h / 20 °C
With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; HATU; lithium hydroxide; Hoveyda-Grubbs catalyst second generation; In tetrahydrofuran; 1,4-dioxane; dichloromethane;
upstream raw materials:

salicylonitrile

1-(3-aminobenzofuran-2-yl)ethan-1-one

C17H13NO2

C19H15NO3

Downstream raw materials:

C44H49N5O9S

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