3-[4-(3,5-dichloro-pyridin-4-yl-methyl)-7-methoxy-phthalazin-1-yl]-phenylamine

Base Information

• Chemical Name: 3-[4-(3,5-dichloro-pyridin-4-yl-methyl)-7-methoxy-phthalazin-1-yl]-phenylamine
• CAS No.: 717107-15-8
• Molecular Formula: C₂₁H₁₆Cl₂N₄O
• Molecular Weight: 411.29

Synonyms:3-[4-(3,5-dichloro-pyridin-4-yl-methyl)-7-methoxy-phthalazin-1-yl]-phenylamine

Chemical Property of 3-[4-(3,5-dichloro-pyridin-4-yl-methyl)-7-methoxy-phthalazin-1-yl]-phenylamine

Chemical Property:

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Technology Process of 3-[4-(3,5-dichloro-pyridin-4-yl-methyl)-7-methoxy-phthalazin-1-yl]-phenylamine

There total 1 articles about 3-[4-(3,5-dichloro-pyridin-4-yl-methyl)-7-methoxy-phthalazin-1-yl]-phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

1-(3,5-dichloro-pyridin-4-ylmethyl)-6-methoxy-4-(3-nitro-phenyl)-phthalazine (717107-14-7) → 3-[4-(3,5-dichloro-pyridin-4-yl-methyl)-7-methoxy-phthalazin-1-yl]-phenylamine (717107-15-8)

Guidance literature:

With hydrogen; platinum(IV) oxide; In 1,4-dioxane; acetic acid; for 8h; under 1034.32 Torr;

Reference yield: 85.0%

3-[4-(3,5-dichloro-pyridin-4-yl-methyl)-7-methoxy-phthalazin-1-yl]-phenylamine (717107-15-8) + 2-Chloroethanesulfonyl chloride (1622-32-8) → C23H19Cl3N4O3S (717107-18-1)

Guidance literature:

With triethylamine; In 1-methyl-pyrrolidin-2-one; at 0 - 20 ℃; for 24h;

Reference yield: 64.0%

glutaric anhydride, (108-55-4) + 3-[4-(3,5-dichloro-pyridin-4-yl-methyl)-7-methoxy-phthalazin-1-yl]-phenylamine (717107-15-8) → 4-{3-[4-(3,5-dichloro-pyridin-4-ylmethyl)-7-methoxy-phthalazin-1-yl]-phenylcarbamoyl}-butyric acid (717107-21-6)

Guidance literature:

In dichloromethane; at 20 - 40 ℃;

upstream raw materials:

1-(3,5-dichloro-pyridin-4-ylmethyl)-6-methoxy-4-(3-nitro-phenyl)-phthalazine

Downstream raw materials:

C₂₃H₁₉Cl₃N₄O₃S

N-{3-[4-(3,5-dichloro-pyridin-4-ylmethyl)-7-methoxy-phthalazin-1-yl]-phenyl}-succinamic acid

4-{3-[4-(3,5-dichloro-pyridin-4-ylmethyl)-7-methoxy-phthalazin-1-yl]-phenylcarbamoyl}-butyric acid

4-{3-[4-(3,5-dichloro-pyridin-4-yl-methyl)-7-methoxy-phthalazin-1-yl]-phenylsulfamoyl}-butyric acid methyl ester

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