allyl [(2S,5R)-4-benzyl-5-(hydroxymethyl)-3,6-dioxopiperazin-2-yl]acetate

Base Information

Chemical Name:allyl [(2S,5R)-4-benzyl-5-(hydroxymethyl)-3,6-dioxopiperazin-2-yl]acetate
CAS No.:1258937-55-1
Molecular Formula:C₁₇H₂₀N₂O₅
Molecular Weight:332.356
Hs Code.:

Synonyms:allyl [(2S,5R)-4-benzyl-5-(hydroxymethyl)-3,6-dioxopiperazin-2-yl]acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl [(2S,5R)-4-benzyl-5-(hydroxymethyl)-3,6-dioxopiperazin-2-yl]acetate

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Technology Process of allyl [(2S,5R)-4-benzyl-5-(hydroxymethyl)-3,6-dioxopiperazin-2-yl]acetate

There total 5 articles about allyl [(2S,5R)-4-benzyl-5-(hydroxymethyl)-3,6-dioxopiperazin-2-yl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: (2S)-4-(allyloxy)-1-{[(2R)-2-(benzylammonio)-3-methoxy-3-oxopropyl]oxy}-1,4-dioxobutan-2-aminium bis(trifluoroacetate)

: 1258937-55-1
allyl [(2S,5R)-4-benzyl-5-(hydroxymethyl)-3,6-dioxopiperazin-2-yl]acetate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In isopropyl alcohol; at 20 ℃; for 40h; Inert atmosphere;
DOI:10.1016/j.tet.2010.10.007

Reference yield:

: C₂HF₃O₂*C₁₈H₂₄N₂O₆

: 1258937-55-1
allyl [(2S,5R)-4-benzyl-5-(hydroxymethyl)-3,6-dioxopiperazin-2-yl]acetate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In isopropyl alcohol; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1002/chem.201200457

Reference yield:

: 1258937-54-0
4-allyl 1-[(2R)-2-(benzylamino)-3-methoxy-3-oxopropyl] N-(tert-butoxycarbonyl)-L-aspartate

: 1258937-55-1
allyl [(2S,5R)-4-benzyl-5-(hydroxymethyl)-3,6-dioxopiperazin-2-yl]acetate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 2 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 18 h / 20 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; In dichloromethane; isopropyl alcohol;
DOI:10.1002/chem.201200457