H{Nb(CO)3PhP(C₂H₄PPh₂)2}

Base Information

Chemical Name:H{Nb(CO)3PhP(C₂H₄PPh₂)2}
CAS No.:93799-64-5
Molecular Formula:C₃₇H₃₄NbO₃P₃
Molecular Weight:712.503
Hs Code.:

H{Nb(CO)3PhP(C<sub>2</sub>H<sub>4</sub>PPh<sub>2</sub>)2}

Synonyms:H{Nb(CO)3PhP(C₂H₄PPh₂)2}

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Chemical Property of H{Nb(CO)3PhP(C₂H₄PPh₂)2}

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Technology Process of H{Nb(CO)3PhP(C₂H₄PPh₂)2}

There total 1 articles about H{Nb(CO)3PhP(C₂H₄PPh₂)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 93800-24-9
cis-[Et₄N][Nb(CO)4(PhP(CH₂CH₂PPh₂)2)]

: 93799-64-5
H{Nb(CO)3PhP(C₂H₄PPh₂)2}

Guidance literature:: With silica gel; In tetrahydrofuran; acetonitrile; byproducts: CO; (N2); complex soln. in THF contg. a few drops of MeCN transferred to silica gel column, eluted with THF; concd., pptd. (pentane); elem. anal.;
DOI:10.1016/0022-328X(84)80629-4

Reference yield: 53.0%

: 93799-64-5
H{Nb(CO)3PhP(C₂H₄PPh₂)2}

: 121097-00-5
{ClNb(CO)3PhP(CH₂CH₂PPh₂)2}

Guidance literature:: With HCl; CO; In tetrahydrofuran; HNb(CO)3PhP(C2H4PPh2)2 reacts in toluene at -78°C with HCl; by warming to room temp. soln. is 40 min stirring under CO, ppt. is filtered and solvent is reduced;

Reference yield:

: 93799-64-5
H{Nb(CO)3PhP(C₂H₄PPh₂)2}

: 108443-50-1
HNb(CO)2((C₆H₅)P(C₂H₄P(C₆H₅)2)2)2

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); (N2 or Ar); Hg lamp; externally irradiated (90 min); pentane added, recrystd. (THF/pentane);
DOI:10.1016/S0022-328X(00)99517-2