3-(2,6-Dichloro-phenyl)-1,2,4,9,10-pentaaza-anthracene 1,2,4-trioxide

Base Information

• Chemical Name: 3-(2,6-Dichloro-phenyl)-1,2,4,9,10-pentaaza-anthracene 1,2,4-trioxide
• CAS No.: 133123-52-1
• Molecular Formula: C₁₅H₇Cl₂N₅O₃
• Molecular Weight: 376.158
• Mol file: 133123-52-1.mol

Synonyms:3-(2,6-Dichloro-phenyl)-1,2,4,9,10-pentaaza-anthracene 1,2,4-trioxide

Chemical Property of 3-(2,6-Dichloro-phenyl)-1,2,4,9,10-pentaaza-anthracene 1,2,4-trioxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(2,6-Dichloro-phenyl)-1,2,4,9,10-pentaaza-anthracene 1,2,4-trioxide

There total 1 articles about 3-(2,6-Dichloro-phenyl)-1,2,4,9,10-pentaaza-anthracene 1,2,4-trioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

<1,2,5>Oxadiazolo<3,4-b>quinoxaline 1-oxide (79421-50-4) + 2,6-dichlorobenzonitrile N-oxide (2904-62-3) → 3-(2,6-Dichloro-phenyl)-1,2,4,9,10-pentaaza-anthracene 1,2,4-trioxide (133123-52-1)

Guidance literature:

In dichloromethane; for 12h; Heating;

DOI:10.1055/s-1991-26387

Reference yield: 72.0%

3-(2,6-Dichloro-phenyl)-1,2,4,9,10-pentaaza-anthracene 1,2,4-trioxide (133123-52-1) → 3-(2,6-Dichloro-phenyl)-9,10-dihydro-1,2,4,9,10-pentaaza-anthracene (133123-56-5)

Guidance literature:

With triphenylphosphine; In chloroform; for 1h; Heating;

DOI:10.1055/s-1991-26387

Reference yield:

3-(2,6-Dichloro-phenyl)-1,2,4,9,10-pentaaza-anthracene 1,2,4-trioxide (133123-52-1) → 3-(2,6-Dichloro-phenyl)-1,2,4,9,10-pentaaza-anthracene (133123-60-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / Ph₃P / CHCl₃ / 1 h / Heating

2: 99 percent / iodosobenzene bis(trifluoroacetate) / CH₂Cl₂ / 0.25 h / Ambient temperature

With triphenylphosphine; bis-[(trifluoroacetoxy)iodo]benzene; In dichloromethane; chloroform;

DOI:10.1055/s-1991-26387

upstream raw materials:

<1,2,5>Oxadiazolo<3,4-b>quinoxaline 1-oxide

2,6-dichlorobenzonitrile N-oxide

Downstream raw materials:

3-(2,6-Dichloro-phenyl)-9,10-dihydro-1,2,4,9,10-pentaaza-anthracene

3-(2,6-Dichloro-phenyl)-1,2,4,9,10-pentaaza-anthracene