β-(o-Acetoxy-phenyl)-propionyl-chlorid

Base Information

Chemical Name:β-(o-Acetoxy-phenyl)-propionyl-chlorid
CAS No.:99854-11-2
Molecular Formula:C₁₁H₁₁ClO₃
Molecular Weight:226.66
Hs Code.:

Synonyms:β-(o-Acetoxy-phenyl)-propionyl-chlorid

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Chemical Property of β-(o-Acetoxy-phenyl)-propionyl-chlorid

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Technology Process of β-(o-Acetoxy-phenyl)-propionyl-chlorid

There total 6 articles about β-(o-Acetoxy-phenyl)-propionyl-chlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17123-74-9
3-[2-(acetyloxy)phenyl]propanoic acid

: 99854-11-2
β-(o-Acetoxy-phenyl)-propionyl-chlorid

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 - 5 ℃; for 0.5h; Inert atmosphere;

Reference yield:

: 495-78-3
3-(2-hydroxyphenyl)propionic acid

: 108-24-7
acetic anhydride

: 99854-11-2
β-(o-Acetoxy-phenyl)-propionyl-chlorid

Guidance literature:: 3-(2-hydroxyphenyl)propionic acid; acetic anhydride; at 80 ℃; for 1h;

With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane; at 20 - 80 ℃; for 2h;

Reference yield:

: 119-84-6,1341-36-2
C₆H₄(CH₂CH₂C(O)O)

: 99854-11-2
β-(o-Acetoxy-phenyl)-propionyl-chlorid

Guidance literature:: Multi-step reaction with 7 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 5 °C / Inert atmosphere

2: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

3: triethylamine; dmap / dichloromethane / 3 h / 0 - 25 °C / Inert atmosphere

4: acetic acid; water / tetrahydrofuran / 3 h / 24 - 25 °C

5: pyridinium chlorochromate / dichloromethane / 2 h / 24 - 25 °C / Inert atmosphere

6: sodium chlorite; sodium dihydrogenphosphate / tert-butyl alcohol; methylbutane / 1 h / 25 - 28 °C / Inert atmosphere

7: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 0.5 h / 0 - 5 °C / Inert atmosphere

With 1H-imidazole; dmap; sodium chlorite; sodium dihydrogenphosphate; lithium aluminium tetrahydride; oxalyl dichloride; water; acetic acid; triethylamine; N,N-dimethyl-formamide; pyridinium chlorochromate; In tetrahydrofuran; methylbutane; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;