Technology Process of C33H54O8Si
There total 23 articles about C33H54O8Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Dess-Martin periodane;
In
dichloromethane;
at 0 - 20 ℃;
for 0.5h;
DOI:10.1021/ol400408w
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium 10% on activated carbon; hydrogen / methanol / 25 h / 20 °C
2: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 47 h / 20 °C
3: Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C
With
palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; Dess-Martin periodane; acetic acid;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ol400408w
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 47 h / 20 °C
2: Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C
With
tetrabutyl ammonium fluoride; Dess-Martin periodane; acetic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ol400408w