dimethyl 1-(3-bromo-4-carbamothioylphenyl)-1H-benzo[d]imidazole-5,6-dicarboxylate

Base Information

Chemical Name:dimethyl 1-(3-bromo-4-carbamothioylphenyl)-1H-benzo[d]imidazole-5,6-dicarboxylate
CAS No.:1093099-01-4
Molecular Formula:C₁₈H₁₄BrN₃O₄S
Molecular Weight:448.297
Hs Code.:

Synonyms:dimethyl 1-(3-bromo-4-carbamothioylphenyl)-1H-benzo[d]imidazole-5,6-dicarboxylate

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Chemical Property of dimethyl 1-(3-bromo-4-carbamothioylphenyl)-1H-benzo[d]imidazole-5,6-dicarboxylate

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Technology Process of dimethyl 1-(3-bromo-4-carbamothioylphenyl)-1H-benzo[d]imidazole-5,6-dicarboxylate

There total 3 articles about dimethyl 1-(3-bromo-4-carbamothioylphenyl)-1H-benzo[d]imidazole-5,6-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1421329-52-3
methyl 3-(1-(3-bromo-4-cyanophenyl)-1H-imidazol-2-yl)propanoate

: 1093099-01-4
dimethyl 1-(3-bromo-4-carbamothioylphenyl)-1H-benzo[d]imidazole-5,6-dicarboxylate

Guidance literature:: With ammonium sulfide; In ethanol; at 90 ℃; for 1.5h; Inert atmosphere;
DOI:10.1016/j.tet.2012.11.070

Reference yield: 75.0%

: 1093099-00-3
dimethyl 1-(3-bromo-4-cyanophenyl)-1H-benzo[d]imidazole-5,6-dicarboxylate

: 1093099-01-4
dimethyl 1-(3-bromo-4-carbamothioylphenyl)-1H-benzo[d]imidazole-5,6-dicarboxylate

Guidance literature:: With tetraphosphorus decasulfide; In ethanol; at 70 ℃; for 20h; Inert atmosphere;
DOI:10.1021/ol8022962

Reference yield:

: 36282-26-5
2-bromo-4-fluorobenzonitrile

: 1093099-01-4
dimethyl 1-(3-bromo-4-carbamothioylphenyl)-1H-benzo[d]imidazole-5,6-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 30 h / 90 °C / Inert atmosphere

2: ammonium sulfide / ethanol / 1.5 h / 90 °C / Inert atmosphere

With ammonium sulfide; N-ethyl-N,N-diisopropylamine; In ethanol; dimethyl sulfoxide;
DOI:10.1016/j.tet.2012.11.070