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Technology Process of C6H5CH2O(CH2)3C11H12O3(CH3)2(OCH2C6H5)(OCHCHCH2Sn(C4H9)3)CH2CH(OCOCH2Cl)OC14H17O5(CH3)2(CHCH2)C6H5

C6H5CH2O(CH2)3C11H12O3(CH3)2(OCH2C6H5)(OCHCHCH2Sn(C4H9)3)CH2CH(OCOCH2Cl)OC14H17O5(CH3)2(CHCH2)C6H5

Base Information
  • Chemical Name:C6H5CH2O(CH2)3C11H12O3(CH3)2(OCH2C6H5)(OCHCHCH2Sn(C4H9)3)CH2CH(OCOCH2Cl)OC14H17O5(CH3)2(CHCH2)C6H5
  • CAS No.:494760-43-9
  • Molecular Formula:C73H105ClO14Sn
  • Molecular Weight:1360.79
  • Hs Code.:
C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>O(CH<sub>2</sub>)3C<sub>11</sub>H<sub>12</sub>O<sub>3</sub>(CH<sub>3</sub>)2(OCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)(OCHCHCH<sub>2</sub>Sn(C<sub>4</sub>H<sub>9</sub>)3)CH<sub>2</sub>CH(OCOCH<sub>2</sub>Cl)OC<sub>14</sub>H<sub>17</sub>O<sub>5</sub>(CH<sub>3</sub>)2(CHCH<sub>2</sub>)C<sub>6</sub>H<sub>5</sub>

Synonyms:C6H5CH2O(CH2)3C11H12O3(CH3)2(OCH2C6H5)(OCHCHCH2Sn(C4H9)3)CH2CH(OCOCH2Cl)OC14H17O5(CH3)2(CHCH2)C6H5

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Chemical Property of C6H5CH2O(CH2)3C11H12O3(CH3)2(OCH2C6H5)(OCHCHCH2Sn(C4H9)3)CH2CH(OCOCH2Cl)OC14H17O5(CH3)2(CHCH2)C6H5
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Technology Process of C6H5CH2O(CH2)3C11H12O3(CH3)2(OCH2C6H5)(OCHCHCH2Sn(C4H9)3)CH2CH(OCOCH2Cl)OC14H17O5(CH3)2(CHCH2)C6H5

There total 1 articles about C6H5CH2O(CH2)3C11H12O3(CH3)2(OCH2C6H5)(OCHCHCH2Sn(C4H9)3)CH2CH(OCOCH2Cl)OC14H17O5(CH3)2(CHCH2)C6H5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>O(CH<sub>2</sub>)3C<sub>11</sub>H<sub>12</sub>O<sub>3</sub>(CH<sub>3</sub>)2(OCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)(OCHCHCH<sub>2</sub>Sn(C<sub>4</sub>H<sub>9</sub>)3)CH<sub>2</sub>CO<sub>2</sub>C<sub>14</sub>H<sub>17</sub>O<sub>5</sub>(CH<sub>3</sub>)2(CHCH<sub>2</sub>)C<sub>6</sub>H<sub>5</sub>

C6H5CH2O(CH2)3C11H12O3(CH3)2(OCH2C6H5)(OCHCHCH2Sn(C4H9)3)CH2CO2C14H17O5(CH3)2(CHCH2)C6H5

acetic anhydride
108-24-7

acetic anhydride

C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>O(CH<sub>2</sub>)3C<sub>11</sub>H<sub>12</sub>O<sub>3</sub>(CH<sub>3</sub>)2(OCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)(OCHCHCH<sub>2</sub>Sn(C<sub>4</sub>H<sub>9</sub>)3)CH<sub>2</sub>CH(OCOCH<sub>2</sub>Cl)OC<sub>14</sub>H<sub>17</sub>O<sub>5</sub>(CH<sub>3</sub>)2(CHCH<sub>2</sub>)C<sub>6</sub>H<sub>5</sub>
494760-43-9

C6H5CH2O(CH2)3C11H12O3(CH3)2(OCH2C6H5)(OCHCHCH2Sn(C4H9)3)CH2CH(OCOCH2Cl)OC14H17O5(CH3)2(CHCH2)C6H5

Guidance literature:
With pyridine; dmap; diisobutylaluminium hydride; In dichloromethane; Rychnovsky protocol; DIBALH, CH2Cl2, -78°C, then O(COCH2Cl)2, DMAP, pyridine, -78°C to room temp.;
DOI:10.1021/ja036984k

Reference yield: 56.0%

C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>O(CH<sub>2</sub>)3C<sub>11</sub>H<sub>12</sub>O<sub>3</sub>(CH<sub>3</sub>)2(OCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)(OCHCHCH<sub>2</sub>Sn(C<sub>4</sub>H<sub>9</sub>)3)CH<sub>2</sub>CH(OCOCH<sub>2</sub>Cl)OC<sub>14</sub>H<sub>17</sub>O<sub>5</sub>(CH<sub>3</sub>)2(CHCH<sub>2</sub>)C<sub>6</sub>H<sub>5</sub>
494760-43-9

C6H5CH2O(CH2)3C11H12O3(CH3)2(OCH2C6H5)(OCHCHCH2Sn(C4H9)3)CH2CH(OCOCH2Cl)OC14H17O5(CH3)2(CHCH2)C6H5

9-[10-benzyloxy-8-(3-benzyloxy-propyl)-10a,11a-dimethyl-2-vinyl-tetradecahydro-1,5,7,11-tetraoxa-naphthacen-3-yloxy]-9,10a-dimethyl-2-phenyl-8-vinyl-dodecahydro-1,3,5,7,11-pentaoxa-benzo[4,5]cyclohepta[1,2-<i>b</i>]naphthalene
494760-38-2

9-[10-benzyloxy-8-(3-benzyloxy-propyl)-10a,11a-dimethyl-2-vinyl-tetradecahydro-1,5,7,11-tetraoxa-naphthacen-3-yloxy]-9,10a-dimethyl-2-phenyl-8-vinyl-dodecahydro-1,3,5,7,11-pentaoxa-benzo[4,5]cyclohepta[1,2-b]naphthalene

9-[10-benzyloxy-8-(3-benzyloxy-propyl)-10a,11a-dimethyl-2-vinyl-tetradecahydro-1,5,7,11-tetraoxa-naphthacen-3-yloxy]-9,10a-dimethyl-2-phenyl-8-vinyl-dodecahydro-1,3,5,7,11-pentaoxa-benzo[4,5]cyclohepta[1,2-<i>b</i>]naphthalene
494760-44-0

9-[10-benzyloxy-8-(3-benzyloxy-propyl)-10a,11a-dimethyl-2-vinyl-tetradecahydro-1,5,7,11-tetraoxa-naphthacen-3-yloxy]-9,10a-dimethyl-2-phenyl-8-vinyl-dodecahydro-1,3,5,7,11-pentaoxa-benzo[4,5]cyclohepta[1,2-b]naphthalene

Guidance literature:
With 4 A molecular sieve; boron trifluoride diethyl etherate; In dichloromethane; acetonitrile; at -40 - 20 ℃; for 4h;
DOI:10.1021/ja036984k
upstream raw materials:

acetic anhydride

Downstream raw materials:

9-[10-benzyloxy-8-(3-benzyloxy-propyl)-10a,11a-dimethyl-2-vinyl-tetradecahydro-1,5,7,11-tetraoxa-naphthacen-3-yloxy]-9,10a-dimethyl-2-phenyl-8-vinyl-dodecahydro-1,3,5,7,11-pentaoxa-benzo[4,5]cyclohepta[1,2-b]naphthalene

9-[10-benzyloxy-8-(3-benzyloxy-propyl)-10a,11a-dimethyl-2-vinyl-tetradecahydro-1,5,7,11-tetraoxa-naphthacen-3-yloxy]-9,10a-dimethyl-2-phenyl-8-vinyl-dodecahydro-1,3,5,7,11-pentaoxa-benzo[4,5]cyclohepta[1,2-b]naphthalene

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