Technology Process of C27H36O6
There total 6 articles about C27H36O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate; Dess-Martin periodane;
In
dichloromethane;
at 0 - 20 ℃;
for 1h;
DOI:10.1002/anie.201403542
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C
1.2: 0 - 20 °C
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 0 - 20 °C
3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C
With
tetrabutyl ammonium fluoride; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane;
In
tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1002/anie.201403542
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: trifluoroacetic acid / pentane / 1 h / -5 °C
1.2: 3 h / 20 °C
2.1: palladium on activated charcoal; hydrogen / methanol / 2 h / 20 °C / Inert atmosphere
3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C
3.2: 0 - 20 °C
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 0 - 20 °C
5.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C
With
palladium on activated charcoal; tetrabutyl ammonium fluoride; hydrogen; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; mineral oil; pentane;
DOI:10.1002/anie.201403542
