1,2-bis(2,6-diisopropylphenyl)disulfane

Base Information

Chemical Name:1,2-bis(2,6-diisopropylphenyl)disulfane
CAS No.:175885-08-2
Molecular Formula:C₂₄H₃₄S₂
Molecular Weight:386.666
Hs Code.:

Synonyms:1,2-bis(2,6-diisopropylphenyl)disulfane

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Chemical Property of 1,2-bis(2,6-diisopropylphenyl)disulfane

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Technology Process of 1,2-bis(2,6-diisopropylphenyl)disulfane

There total 3 articles about 1,2-bis(2,6-diisopropylphenyl)disulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 24010-52-4
S-(2,6-diisopropylphenyl)dimethylcarbamothioate

: 175885-08-2
1,2-bis(2,6-diisopropylphenyl)disulfane

: 91638-62-9
2,6-diisopropyl phenylthiol

Guidance literature:: With lithium aluminium tetrahydride; In 1,2-dimethoxyethane; for 4h; Inert atmosphere; Cooling with ice; Reflux;
DOI:10.1021/jo402791c

Reference yield:

: 2078-54-8
2,6-diisopropylphenol

: 175885-08-2
1,2-bis(2,6-diisopropylphenyl)disulfane

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / 1-methyl-pyrrolidin-2-one; mineral oil / 0.5 h / 20 °C / Inert atmosphere; Cooling with ice

1.2: 1 h / 80 °C / Inert atmosphere

2.1: 1 h / 260 °C

3.1: lithium aluminium tetrahydride / 1,2-dimethoxyethane / 4 h / Inert atmosphere; Cooling with ice; Reflux

With lithium aluminium tetrahydride; sodium hydride; In 1-methyl-pyrrolidin-2-one; 1,2-dimethoxyethane; mineral oil; 2.1: |Newman-Kwart Rearrangement;
DOI:10.1021/jo402791c

Reference yield:

: 24010-73-9
O-2,6-di-isopropylphenyl N,N-dimethylthiocarbamate

: 175885-08-2
1,2-bis(2,6-diisopropylphenyl)disulfane

Guidance literature:: Multi-step reaction with 2 steps

1: 1 h / 260 °C

2: lithium aluminium tetrahydride / 1,2-dimethoxyethane / 4 h / Inert atmosphere; Cooling with ice; Reflux

With lithium aluminium tetrahydride; In 1,2-dimethoxyethane; 1: |Newman-Kwart Rearrangement;
DOI:10.1021/jo402791c