N-benzyl-4-bromo-3-chloro-N-(2-oxopropyl)-1,2-dihydrocyclobutabenzene-1-carboxamide

Base Information

Chemical Name:N-benzyl-4-bromo-3-chloro-N-(2-oxopropyl)-1,2-dihydrocyclobutabenzene-1-carboxamide
CAS No.:1135491-01-8
Molecular Formula:C₁₉H₁₇BrClNO₂
Molecular Weight:406.706
Hs Code.:

Synonyms:N-benzyl-4-bromo-3-chloro-N-(2-oxopropyl)-1,2-dihydrocyclobutabenzene-1-carboxamide

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Chemical Property of N-benzyl-4-bromo-3-chloro-N-(2-oxopropyl)-1,2-dihydrocyclobutabenzene-1-carboxamide

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Technology Process of N-benzyl-4-bromo-3-chloro-N-(2-oxopropyl)-1,2-dihydrocyclobutabenzene-1-carboxamide

There total 1 articles about N-benzyl-4-bromo-3-chloro-N-(2-oxopropyl)-1,2-dihydrocyclobutabenzene-1-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1135490-97-9
N-benzyl-4-bromo-3-chloro-N-(2-hydroxypropyl)-1,2-dihydrocyclobutabenzene-1-carboxamide

: 1135491-01-8
N-benzyl-4-bromo-3-chloro-N-(2-oxopropyl)-1,2-dihydrocyclobutabenzene-1-carboxamide

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 2.25h;

Reference yield: 19.0%

: 1135491-01-8
N-benzyl-4-bromo-3-chloro-N-(2-oxopropyl)-1,2-dihydrocyclobutabenzene-1-carboxamide

: cis-2-benzyl-7-bromo-6-chloro-3a-methyl-3,3a,5,9b-tetrahydroisochromeno[3,4-c]pyrrol-1(2H)-one

: trans-2-benzyl-7-bromo-6-chloro-3a-methyl-3,3a,5,9b-tetrahydroisochromeno[3,4-c]pyrrol-1(2H)-one

Guidance literature:: In bromobenzene; at 210 ℃; for 0.5h; Microwave heating;

Reference yield:

: 1135491-01-8
N-benzyl-4-bromo-3-chloro-N-(2-oxopropyl)-1,2-dihydrocyclobutabenzene-1-carboxamide

: C₁₉H₁₇BrClNO₂

: C₁₉H₁₇BrClNO₂

Guidance literature:: In bromobenzene; at 210 ℃; for 0.5h; optical yield given as %de; diastereoselective reaction; Microwave irradiation;
DOI:10.1016/j.tetlet.2011.03.055