Cr(η6-1,3,5-Me3C6H3)2Br

Base Information

• Chemical Name: Cr(η6-1,3,5-Me3C6H3)2Br
• CAS No.: 945910-54-3
• Molecular Formula: Br*C₁₈H₂₄Cr
• Molecular Weight: 372.289
• Mol file: 945910-54-3.mol

Synonyms:Cr(η6-1,3,5-Me3C6H3)2Br

Chemical Property of Cr(η6-1,3,5-Me3C6H3)2Br

Chemical Property:

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Technology Process of Cr(η6-1,3,5-Me3C6H3)2Br

There total 1 articles about Cr(η6-1,3,5-Me3C6H3)2Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

cobaltocenium bromide + bis(η-mesitylene)chromium(0) (1274-07-3) → cobaltocene (1277-43-6,78206-33-4) + Cr(η6-1,3,5-Me3C6H3)2Br (945910-54-3)

Guidance literature:

In tetrahydrofuran; (under Ar); soln. of Cr-complex in THF treated with Co-complex, stirred for 12 h at room temp.; ppt. filtered, washed with THF, dried in vacuo at room temp., vol. of mother liquor reduced, heptane added, filtered, dried in vacuo;

DOI:10.1016/j.jorganchem.2007.01.044

upstream raw materials:

bis(η-mesitylene)chromium(0)

Refernces