C₁₉H₂₀F₆N₄O₄

Base Information

Chemical Name:C₁₉H₂₀F₆N₄O₄
CAS No.:1400917-14-7
Molecular Formula:C₁₉H₂₀F₆N₄O₄
Molecular Weight:482.383
Hs Code.:

C<sub>19</sub>H<sub>20</sub>F<sub>6</sub>N<sub>4</sub>O<sub>4</sub>

Synonyms:C₁₉H₂₀F₆N₄O₄

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Chemical Property of C₁₉H₂₀F₆N₄O₄

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Technology Process of C₁₉H₂₀F₆N₄O₄

There total 5 articles about C₁₉H₂₀F₆N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1400917-10-3
C₁₂H₁₆F₃N₃O₄

: 1535-73-5
m-trifluoromethoxyaniline

: 1400917-14-7
C₁₉H₂₀F₆N₄O₄

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 80 ℃;
DOI:10.1016/j.tet.2012.07.069

Reference yield:

: 1400916-92-8
C₁₇H₁₇F₃N₂O₄

: 1400917-14-7
C₁₉H₂₀F₆N₄O₄

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen; 10% Pd/C / ethyl acetate / 6 h / 20 °C

2: triethylamine; diphenyl phosphoryl azide / 8 h / 83 °C

3: lithium hydroxide; water / tetrahydrofuran / 72 h / 20 °C

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 80 °C

With diphenyl phosphoryl azide; 10% Pd/C; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; 2: |Curtius Rearrangement;
DOI:10.1016/j.tet.2012.07.069

Reference yield:

: 1400917-09-0
C₁₄H₂₀F₃N₃O₄

: 1400917-14-7
C₁₉H₂₀F₆N₄O₄

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide; water / tetrahydrofuran / 72 h / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 80 °C

With water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.07.069