cHDMS-H-ADT

Base Information

Chemical Name:cHDMS-H-ADT
CAS No.:1363396-34-2
Molecular Formula:C₃₈H₄₂S₂Si₂
Molecular Weight:619.054
Hs Code.:

Synonyms:cHDMS-H-ADT

Suppliers and Price of cHDMS-H-ADT

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cHDMS-H-ADT

Chemical Property:

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Technology Process of cHDMS-H-ADT

There total 2 articles about cHDMS-H-ADT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: ethynylcyclohexyldimethylsilane

: 143746-72-9
dithieno<2,3-b><6,7-d>-9,10-anthraquinone

: 1363396-34-2
cHDMS-H-ADT

Guidance literature:: ethynylcyclohexyldimethylsilane; With n-butyllithium; In 1,4-dioxane; hexanes; at 0 - 20 ℃; for 1.5h; Inert atmosphere;

dithieno<2,3-b><6,7-d>-9,10-anthraquinone; In 1,4-dioxane; hexanes; at 20 - 50 ℃; for 19h;

With hydrogenchloride; tin(ll) chloride; In 1,4-dioxane; hexanes; water; at 20 ℃; for 0.666667h; Darkness;

Reference yield:

: 71864-47-6
chloro-cyclohexyl-dimethylsilane

: 1363396-34-2
cHDMS-H-ADT

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 1 h / 20 - 50 °C

1.2: 0.08 h / Cooling with ice

2.1: n-butyllithium / 1,4-dioxane; hexanes / 1.5 h / 0 - 20 °C / Inert atmosphere

2.2: 19 h / 20 - 50 °C

2.3: 0.67 h / 20 °C / Darkness

With n-butyllithium; In tetrahydrofuran; 1,4-dioxane; hexanes;