C₃₃H₅₂O₆Si

Base Information Edit

Chemical Name:C₃₃H₅₂O₆Si
CAS No.:1206911-17-2
Molecular Formula:C₃₃H₅₂O₆Si
Molecular Weight:572.858
Hs Code.:
Mol file:1206911-17-2.mol

C<sub>33</sub>H<sub>52</sub>O<sub>6</sub>Si

Synonyms:C₃₃H₅₂O₆Si

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Chemical Property of C₃₃H₅₂O₆Si Edit

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Technology Process of C₃₃H₅₂O₆Si

There total 2 articles about C₃₃H₅₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 486-21-5
isofraxidin

: 1206911-12-7
C₂₂H₄₄O₂Si

: 1206911-17-2
C₃₃H₅₂O₆Si

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 25 ℃; for 2h;
DOI:10.1002/ejoc.200901021

Reference yield:

: 1206911-05-8
C₁₇H₂₈O₂

: 1206911-17-2
C₃₃H₅₂O₆Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride

2.1: tert-butyldimethylsilyl chloride

3.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 3 h / 25 °C / Inert atmosphere

3.2: 1 h / 25 °C / Inert atmosphere

4.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 25 °C

With lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; tert-butyldimethylsilyl chloride; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; In tetrahydrofuran; 4.1: Mitsunobu reaction;
DOI:10.1002/ejoc.200901021