3-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2,6-dimethoxyphenyl chloroacetate

Base Information

Chemical Name:3-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2,6-dimethoxyphenyl chloroacetate
CAS No.:1344112-12-4
Molecular Formula:C₂₂H₂₃ClO₁₀
Molecular Weight:482.872
Hs Code.:

Synonyms:3-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2,6-dimethoxyphenyl chloroacetate

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Chemical Property of 3-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2,6-dimethoxyphenyl chloroacetate

Chemical Property:

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Technology Process of 3-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2,6-dimethoxyphenyl chloroacetate

There total 2 articles about 3-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2,6-dimethoxyphenyl chloroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 18780-67-1
4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoic acid

: 1440-81-9
2,6-dimethoxyphenyl chloroacetate

: 1344112-12-4
3-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2,6-dimethoxyphenyl chloroacetate

Guidance literature:: With eaton’s reagent; at 60 ℃;
DOI:10.1016/j.bioorg.2020.103643

Reference yield:

: 91-10-1
1,3-dimethoxy-2-hydroxy-benzene

: 1344112-12-4
3-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2,6-dimethoxyphenyl chloroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 7 h / 135 °C / Inert atmosphere

2: methanesulfonic acid; phosphorus pentoxide / 3 h / 50 °C / Inert atmosphere

With methanesulfonic acid; phosphorus pentoxide; 2: Friedel Crafts acylation;
DOI:10.1016/j.bmc.2011.08.047

Reference yield:

: 1344112-12-4
3-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2,6-dimethoxyphenyl chloroacetate

: 50389-19-0
(3-hydroxy-2,4-dimethoxyphenyl)(4-hydroxy-3,5-dimethoxyphenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium acetate / methanol / 1 h / Reflux

2: ethanolamine / ethanol / 5 h / 20 °C

With water; sodium acetate; ethanolamine; In methanol; ethanol;
DOI:10.1016/j.bmc.2011.08.047