(6R,7R)-3-(1-Methyl-1H-tetrazol-5-ylsulfanylmethyl)-8-oxo-7-(2-oxo-2-phenyl-acetylamino)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzyl ester

Base Information

Chemical Name:(6R,7R)-3-(1-Methyl-1H-tetrazol-5-ylsulfanylmethyl)-8-oxo-7-(2-oxo-2-phenyl-acetylamino)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzyl ester
CAS No.:91530-75-5
Molecular Formula:C₂₅H₂₂N₆O₅S₂
Molecular Weight:550.619
Hs Code.:

(6R,7R)-3-(1-Methyl-1H-tetrazol-5-ylsulfanylmethyl)-8-oxo-7-(2-oxo-2-phenyl-acetylamino)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzyl ester

Synonyms:(6R,7R)-3-(1-Methyl-1H-tetrazol-5-ylsulfanylmethyl)-8-oxo-7-(2-oxo-2-phenyl-acetylamino)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzyl ester

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Chemical Property of (6R,7R)-3-(1-Methyl-1H-tetrazol-5-ylsulfanylmethyl)-8-oxo-7-(2-oxo-2-phenyl-acetylamino)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzyl ester

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Technology Process of (6R,7R)-3-(1-Methyl-1H-tetrazol-5-ylsulfanylmethyl)-8-oxo-7-(2-oxo-2-phenyl-acetylamino)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzyl ester

There total 7 articles about (6R,7R)-3-(1-Methyl-1H-tetrazol-5-ylsulfanylmethyl)-8-oxo-7-(2-oxo-2-phenyl-acetylamino)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 91775-99-4
(R)-2-[(2R,3R)-2-(Benzothiazol-2-yldisulfanyl)-4-oxo-3-(2-oxo-2-phenyl-acetylamino)-azetidin-1-yl]-3-(1-methyl-1H-tetrazol-5-ylsulfanylmethyl)-but-3-enoic acid benzyl ester

: 91530-75-5
(6R,7R)-3-(1-Methyl-1H-tetrazol-5-ylsulfanylmethyl)-8-oxo-7-(2-oxo-2-phenyl-acetylamino)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzyl ester

Guidance literature:: With ammonia; In N,N-dimethyl-formamide; at -30 ℃; for 0.25h;
DOI:10.1016/S0040-4039(01)90045-0

Reference yield:

: 91530-64-2
(R)-2-((1R,5R)-3-Benzoyl-7-oxo-4-thia-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-methyl-but-3-enoic acid benzyl ester

: 91530-75-5
(6R,7R)-3-(1-Methyl-1H-tetrazol-5-ylsulfanylmethyl)-8-oxo-7-(2-oxo-2-phenyl-acetylamino)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / NaCl, H₂SO₄ / CHCl₃; 2-methyl-propan-2-ol; H₂O / electrolytic chlorination

2: NaI / acetone / Heating

3: acetone

4: 78 percent / aqueous 10percent HClO₄ / tetrahydrofuran / 50 h / Ambient temperature

5: 100 percent / NH₃ / dimethylformamide / 0.25 h / -30 °C

With perchloric acid; sulfuric acid; ammonia; sodium iodide; sodium chloride; In tetrahydrofuran; chloroform; water; N,N-dimethyl-formamide; acetone; tert-butyl alcohol;
DOI:10.1016/S0040-4039(01)90045-0

Reference yield:

: 91530-65-3
(R)-2-((1R,5R)-3-Benzoyl-7-oxo-4-thia-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-chloromethyl-but-3-enoic acid benzyl ester

: 91530-75-5
(6R,7R)-3-(1-Methyl-1H-tetrazol-5-ylsulfanylmethyl)-8-oxo-7-(2-oxo-2-phenyl-acetylamino)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: NaI / acetone / Heating

2: acetone

3: 78 percent / aqueous 10percent HClO₄ / tetrahydrofuran / 50 h / Ambient temperature

4: 100 percent / NH₃ / dimethylformamide / 0.25 h / -30 °C

With perchloric acid; ammonia; sodium iodide; In tetrahydrofuran; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4039(01)90045-0