N'-(1-(1-Hydroxy-1lambda(5)-pyridin-2-yl)ethylidene)-1-azepanecarbothiohydrazide

Base Information

Chemical Name:N'-(1-(1-Hydroxy-1lambda(5)-pyridin-2-yl)ethylidene)-1-azepanecarbothiohydrazide
CAS No.:87587-04-0
Molecular Formula:C₁₄H₂₀N₄OS
Molecular Weight:292.405
Hs Code.:
UNII:U7B5QVY7PW

Synonyms:NSC 351075;87587-04-0;N'-(1-(1-Hydroxy-1lambda(5)-pyridin-2-yl)ethylidene)-1-azepanecarbothiohydrazide;NSC351075;NSC-351075;U7B5QVY7PW;NCI60_003130;1H-Azepine-1-carbothioic acid, hexahydro-, [1-(1-oxido-2-pyridinyl)ethylidene]hydrazide;1H-Azepine-1-carbothioic acid, hexahydro-, [1-(2-pyridinyl)ethylidene]hydrazide, N-oxide;1H-Azepine-1-carbothioic acid, hexahydro-, 2-[1-(1-oxido-2-pyridinyl)ethylidene]hydrazide;Hexahydro-1H-azepine-1-carbothioic acid 2-[1-(1-oxido-2-pyridinyl)ethylidene]hydrazide;N-[(E)-1-(1-oxidopyridin-1-ium-2-yl)ethylideneamino]azepane-1-carbothioamide

Suppliers and Price of N'-(1-(1-Hydroxy-1lambda(5)-pyridin-2-yl)ethylidene)-1-azepanecarbothiohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N'-(1-(1-Hydroxy-1lambda(5)-pyridin-2-yl)ethylidene)-1-azepanecarbothiohydrazide

Chemical Property:

Vapor Pressure:1.87E-08mmHg at 25°C
Boiling Point:410.5°Cat760mmHg
Flash Point:202.1°C
Density:1.23g/cm³
XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:292.13578245
Heavy Atom Count:20
Complexity:474

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=C1C=CC=CN1O)N=NC(=S)N2CCCCCC2
Isomeric SMILES:C/C(=C\1/C=CC=CN1O)/N=NC(=S)N2CCCCCC2

Technology Process of N'-(1-(1-Hydroxy-1lambda(5)-pyridin-2-yl)ethylidene)-1-azepanecarbothiohydrazide

There total 2 articles about N'-(1-(1-Hydroxy-1lambda(5)-pyridin-2-yl)ethylidene)-1-azepanecarbothiohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 111-49-9
hexamethylene imine

: 87587-00-6
methyl 3-<1-(2-pyridinyl 1-oxide)ethylidene>hydrazinecarbodithioate

: 87587-04-0
Azepane-1-carbothioic acid [1-(1-oxy-pyridin-2-yl)-eth-(E)-ylidene]-hydrazide

Guidance literature:: In methanol; for 6h; Heating;
DOI:10.1021/jm00367a019

Reference yield:

: 2457-50-3
2-acetylpyridine N-oxide

: 87587-04-0
Azepane-1-carbothioic acid [1-(1-oxy-pyridin-2-yl)-eth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / methanol / 0.5 h / 50 °C

2: 92 percent / methanol / 6 h / Heating

In methanol;
DOI:10.1021/jm00367a019