3,7-anhydro-6-C-<5,9-anhydro-6,7,10-tri-O-benzyl-8-C-(bromoethynyl)-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-D-glycero-D-gulo-decitol-1-yl>-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-ylo...

Base Information

• Chemical Name: 3,7-anhydro-6-C-<5,9-anhydro-6,7,10-tri-O-benzyl-8-C-(bromoethynyl)-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-D-glycero-D-gulo-decitol-1-yl>-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-ylo...
• CAS No.: 176094-16-9
• Molecular Formula: C₇₄H₈₁BrO₁₀Si
• Molecular Weight: 1238.44

Synonyms:3,7-anhydro-6-C-<5,9-anhydro-6,7,10-tri-O-benzyl-8-C-(bromoethynyl)-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-D-glycero-D-gulo-decitol-1-yl>-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-ylo...

Chemical Property of 3,7-anhydro-6-C-<5,9-anhydro-6,7,10-tri-O-benzyl-8-C-(bromoethynyl)-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-D-glycero-D-gulo-decitol-1-yl>-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-ylo...

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Technology Process of 3,7-anhydro-6-C-<5,9-anhydro-6,7,10-tri-O-benzyl-8-C-(bromoethynyl)-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-D-glycero-D-gulo-decitol-1-yl>-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-ylo...

There total 2 articles about 3,7-anhydro-6-C-<5,9-anhydro-6,7,10-tri-O-benzyl-8-C-(bromoethynyl)-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-D-glycero-D-gulo-decitol-1-yl>-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-ylo... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3,7-anhydro-6C-<5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-<(trimethylgermyl)ethynyl>-D-glycero-D-gulo-decitol-1-yl>-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-... → 3,7-anhydro-6-C-<5,9-anhydro-6,7,10-tri-O-benzyl-8-C-(bromoethynyl)-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-D-glycero-D-gulo-decitol-1-yl>-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-ylo... (176094-16-9)

Guidance literature:

With N-Bromosuccinimide; silver trifluoroacetate; In acetone; for 2h; Ambient temperature;

DOI:10.1002/hlca.19960790126

Reference yield: 94.0%

3,7-anhydro-6-C-(5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-ethynyl-D-glycero-D-gulo-decitol-1-yl)-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-yloxy)...>> (170474-92-7) → 3,7-anhydro-6-C-<5,9-anhydro-6,7,10-tri-O-benzyl-8-C-(bromoethynyl)-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-D-glycero-D-gulo-decitol-1-yl>-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-ylo... (176094-16-9)

Guidance literature:

With N-Bromosuccinimide; silver trifluoroacetate; In acetone; for 2h; Ambient temperature;

DOI:10.1002/hlca.19960790126

Reference yield:

3,7-anhydro-6-C-<5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-<(trimethylsilyl)ethynyl>-D-glycero-D-gulo-decitol-1-yl>-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<(3-hydroxy-1,1-dimethylpropyl)...> + 3,7-anhydro-6-C-<5,9-anhydro-6,7,10-tri-O-benzyl-8-C-(bromoethynyl)-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-D-glycero-D-gulo-decitol-1-yl>-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-ylo... (176094-16-9) → C139H146O18Si2

Guidance literature:

With 1,2,2,6,6-pentamethylpiperidine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; In dimethyl sulfoxide; for 10h; Yield given; Ambient temperature;

DOI:10.1002/hlca.19960790126

upstream raw materials:

3,7-anhydro-6-C-(5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-ethynyl-D-glycero-D-gulo-decitol-1-yl)-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-yloxy)...>>

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