Technology Process of C44H66O9SSi
There total 22 articles about C44H66O9SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/ol2007296
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dichloromethane / 15 h / -78 - 20 °C / Inert atmosphere
2: dihydrogen peroxide / methanol; dichloromethane; water / 1 h / 0 °C / Inert atmosphere
3: Inert atmosphere
4: lithium hydroperoxide / Inert atmosphere
5: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
With
lithium hydroperoxide; dihydrogen peroxide; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; dichloromethane; water;
1: Aldol condensation / 5: Mitsunobu reaction;
DOI:10.1021/ol2007296
- Guidance literature:
-
Multi-step reaction with 3 steps
1: water; calcium carbonate; methyl iodide / acetonitrile / 15 h / 40 °C / Inert atmosphere
2: samarium diiodide / tetrahydrofuran; methanol / 0.5 h / -10 °C / Inert atmosphere
3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
With
samarium diiodide; water; triphenylphosphine; calcium carbonate; diethylazodicarboxylate; methyl iodide;
In
tetrahydrofuran; methanol; acetonitrile;
3: Mitsunobu reaction;
DOI:10.1021/ol2007296
