3,3'-bis[4,7,10-trioxatridecaneiminocarbonyl]bis(benzoic acid methyl ester)

Base Information

Chemical Name:3,3'-bis[4,7,10-trioxatridecaneiminocarbonyl]bis(benzoic acid methyl ester)
CAS No.:180294-07-9
Molecular Formula:C₂₈H₃₆N₂O₉
Molecular Weight:544.602
Hs Code.:

Synonyms:3,3'-bis[4,7,10-trioxatridecaneiminocarbonyl]bis(benzoic acid methyl ester)

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Chemical Property of 3,3'-bis[4,7,10-trioxatridecaneiminocarbonyl]bis(benzoic acid methyl ester)

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Technology Process of 3,3'-bis[4,7,10-trioxatridecaneiminocarbonyl]bis(benzoic acid methyl ester)

There total 1 articles about 3,3'-bis[4,7,10-trioxatridecaneiminocarbonyl]bis(benzoic acid methyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 4246-51-9
4,7,10-trioxa-1,13-diaminotridecane

: 3441-03-0
3-(methoxycarbonyl)benzoyl chloride

: 180294-07-9
3,3'-bis[4,7,10-trioxatridecaneiminocarbonyl]bis(benzoic acid methyl ester)

Guidance literature:: With triethylamine; In dichloromethane; for 12h; Ambient temperature;

Reference yield:

: 180294-07-9
3,3'-bis[4,7,10-trioxatridecaneiminocarbonyl]bis(benzoic acid methyl ester)

: 180294-01-3
3,3'-bis[4,7,10-trioxatridecaneiminocarbonyl]bis(benzoyl chloride)

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / methanol / 20 h / Heating

2: SOCl₂ / dimethylformamide / 7.5 h / Heating

With sodium hydroxide; thionyl chloride; In methanol; N,N-dimethyl-formamide;