3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-N-phthalamido-β-D-glucopyranosyl-1’,1’,1’-trichloroacetimidate

Base Information

Chemical Name:3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-N-phthalamido-β-D-glucopyranosyl-1’,1’,1’-trichloroacetimidate
CAS No.:218961-09-2
Molecular Formula:C₃₀H₂₅Cl₃N₂O₇
Molecular Weight:631.897
Hs Code.:

Synonyms:3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-N-phthalamido-β-D-glucopyranosyl-1’,1’,1’-trichloroacetimidate

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Chemical Property of 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-N-phthalamido-β-D-glucopyranosyl-1’,1’,1’-trichloroacetimidate

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Technology Process of 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-N-phthalamido-β-D-glucopyranosyl-1’,1’,1’-trichloroacetimidate

There total 12 articles about 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-N-phthalamido-β-D-glucopyranosyl-1’,1’,1’-trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129575-88-8
p-Methoxyphenyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 545-06-2
trichloroacetonitrile

: 218961-09-2
3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-N-phthalamido-β-D-glucopyranosyl-1’,1’,1’-trichloroacetimidate

: 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-α,β-D-glucopyranosyl trichloroacetimidate

Guidance literature:: p-Methoxyphenyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside; With ammonium cerium (IV) nitrate; In water; acetonitrile; at 0 ℃; for 3h;

trichloroacetonitrile; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 2h; Overall yield = 70 percent; Overall yield = 1.524 g;