dihydrocholesteryl-2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

Base Information

Chemical Name:dihydrocholesteryl-2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside
CAS No.:278800-64-9
Molecular Formula:C₆₁H₇₄O₁₀
Molecular Weight:967.253
Hs Code.:

Synonyms:dihydrocholesteryl-2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

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Chemical Property of dihydrocholesteryl-2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

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Technology Process of dihydrocholesteryl-2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

There total 2 articles about dihydrocholesteryl-2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 80-97-7
Cholestanol

: 64768-20-3,66530-18-5,113544-55-1,121530-16-3,121530-28-7,135216-27-2,101857-05-0
2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

: 278800-64-9
dihydrocholesteryl-2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

Guidance literature:: 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside; With trifluoromethylsulfonic anhydride; 1,1'-sulfinylbisbenzene; In dichloromethane; toluene; at -78 - -40 ℃; for 1.1h;

Cholestanol; With 2-chloropyridine; In dichloromethane; toluene; at -40 - 23 ℃; for 2.5h; Further stages.;
DOI:10.1021/ja993595a

Reference yield: 76.0%

: 80-97-7
Cholestanol

: 183901-63-5
2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

: 278800-64-9
dihydrocholesteryl-2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

Guidance literature:: Cholestanol; 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate; In dichloromethane; at 0 ℃; for 0.5h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1.5h;