1,2-O-isopropylidene-5-O-benzoyl-3-O-trifluoromethanesulfonyl-α-D-ribofuranose

Base Information

Chemical Name:1,2-O-isopropylidene-5-O-benzoyl-3-O-trifluoromethanesulfonyl-α-D-ribofuranose
CAS No.:1356929-41-3
Molecular Formula:C₁₆H₁₇F₃O₈S
Molecular Weight:426.367
Hs Code.:

Synonyms:1,2-O-isopropylidene-5-O-benzoyl-3-O-trifluoromethanesulfonyl-α-D-ribofuranose

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Chemical Property of 1,2-O-isopropylidene-5-O-benzoyl-3-O-trifluoromethanesulfonyl-α-D-ribofuranose

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Technology Process of 1,2-O-isopropylidene-5-O-benzoyl-3-O-trifluoromethanesulfonyl-α-D-ribofuranose

There total 1 articles about 1,2-O-isopropylidene-5-O-benzoyl-3-O-trifluoromethanesulfonyl-α-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 6612-91-5
((3aR,5R,65,6aR)-6-hydroxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methyl benzoate

: 358-23-6
trifluoromethylsulfonic anhydride

: 1356929-41-3
1,2-O-isopropylidene-5-O-benzoyl-3-O-trifluoromethanesulfonyl-α-D-ribofuranose

Guidance literature:: With pyridine; In dichloromethane; at -15 ℃; for 2h;
DOI:10.1039/c1cc13300d

Reference yield: 47.0%

: 1356929-41-3
1,2-O-isopropylidene-5-O-benzoyl-3-O-trifluoromethanesulfonyl-α-D-ribofuranose

: 108-98-5
thiophenol

: 1332508-11-8
1,2-O-isopropylidene-3-phenylsulfanyl-3-deoxy-α-D-xylofuranose

: 1332508-10-7
1,2-O-isopropylidene-5-O-benzoyl-3-phenylsulfanyl-3-deoxy-α-D-xylofuranose

Guidance literature:: thiophenol; With sodium hydride; In tetrahydrofuran; for 0.0333333h;

1,2-O-isopropylidene-5-O-benzoyl-3-O-trifluoromethanesulfonyl-α-D-ribofuranose; In tetrahydrofuran; at -78 ℃; for 1.5h;
DOI:10.1039/c1cc13300d

Reference yield:

: 1356929-41-3
1,2-O-isopropylidene-5-O-benzoyl-3-O-trifluoromethanesulfonyl-α-D-ribofuranose

: 1332508-19-6
C₄₂H₅₇O₆PS

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0.03 h

1.2: 1.5 h / -78 °C

2.1: ammonia / methanol; water / 20 °C

3.1: pyridine / toluene / 1.5 h / 80 °C

With pyridine; ammonia; sodium hydride; In tetrahydrofuran; methanol; water; toluene;
DOI:10.1039/c1cc13300d