(Z)-3-iodo-1-[iodo(phenyl)methylene]-5,6-bis(octyloxy)-2-phenyl-1H-indene

Base Information

Chemical Name:(Z)-3-iodo-1-[iodo(phenyl)methylene]-5,6-bis(octyloxy)-2-phenyl-1H-indene
CAS No.:1616078-69-3
Molecular Formula:C₃₈H₄₆I₂O₂
Molecular Weight:788.591
Hs Code.:

Synonyms:(Z)-3-iodo-1-[iodo(phenyl)methylene]-5,6-bis(octyloxy)-2-phenyl-1H-indene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3-iodo-1-[iodo(phenyl)methylene]-5,6-bis(octyloxy)-2-phenyl-1H-indene

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Technology Process of (Z)-3-iodo-1-[iodo(phenyl)methylene]-5,6-bis(octyloxy)-2-phenyl-1H-indene

There total 3 articles about (Z)-3-iodo-1-[iodo(phenyl)methylene]-5,6-bis(octyloxy)-2-phenyl-1H-indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616078-56-8
4,5-bis(octyloxy)-1,2-bis(phenylethynyl)benzene

: 1616078-69-3
(Z)-3-iodo-1-[iodo(phenyl)methylene]-5,6-bis(octyloxy)-2-phenyl-1H-indene

: 1616078-63-7
(E)-3-iodo-1-[iodo(phenyl)methylene]-5,6-bis(octyloxy)-2-phenyl-1H-indene

Guidance literature:: With iodine; In chloroform; at 20 ℃; for 12h; Overall yield = 95 %; Overall yield = 1.82 g; Inert atmosphere;
DOI:10.1021/ol5015366

Reference yield:

: 248277-14-7
1,2-diiodo-4,5-bis(octyloxy)benzene

: 1616078-69-3
(Z)-3-iodo-1-[iodo(phenyl)methylene]-5,6-bis(octyloxy)-2-phenyl-1H-indene

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisopropylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / Inert atmosphere

1.2: Inert atmosphere

2.1: diisopropylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 48 h / 20 °C / Inert atmosphere

3.1: iodine / chloroform / 12 h / 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; iodine; diisopropylamine; In chloroform;
DOI:10.1021/ol5015366

Reference yield:

: 591-50-4
iodobenzene

: 1,2-diethynyl-4,5-bis(octyloxy)benzene

: 1616078-69-3
(Z)-3-iodo-1-[iodo(phenyl)methylene]-5,6-bis(octyloxy)-2-phenyl-1H-indene

Guidance literature:: Multi-step reaction with 2 steps

1: diisopropylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 48 h / 20 °C / Inert atmosphere

2: iodine / chloroform / 12 h / 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; iodine; diisopropylamine; In chloroform;
DOI:10.1021/ol5015366