C₆₉H₉₄N₂SiO₁₆

Base Information

Chemical Name:C₆₉H₉₄N₂SiO₁₆
CAS No.:944064-71-5
Molecular Formula:C₆₉H₉₄N₂O₁₆Si
Molecular Weight:1235.59
Hs Code.:

C<sub>69</sub>H<sub>94</sub>N<sub>2</sub>SiO<sub>16</sub>

Synonyms:C₆₉H₉₄N₂SiO₁₆

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Chemical Property of C₆₉H₉₄N₂SiO₁₆

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Technology Process of C₆₉H₉₄N₂SiO₁₆

There total 6 articles about C₆₉H₉₄N₂SiO₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-O-acetyl-3,4,6-tri-O-benzyl-D-galactopyranosyl trichloroacetimidate

: 944064-71-5
C₆₉H₉₄N₂SiO₁₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: 75 percent / tin (II) triflate / CH₂Cl₂; acetonitrile / 0 °C

2.1: sodium methanolate / methanol

3.1: 1.4 g / sodium hydride / dimethylformamide / 16 h

4.1: conc. nitric acid; acetic anhydride / CH₂Cl₂ / 1 h / -30 °C

4.2: 68 percent / triethylamine / CH₂Cl₂ / 0.42 h

5.1: potassium tert-butoxide / toluene / 2 h

With potassium tert-butylate; nitric acid; sodium methylate; acetic anhydride; sodium hydride; tin (II) triflate; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/jo061670b

Reference yield:

: 166021-01-8
1,5-anhydro-6-O-triisopropylsilyl-2-deoxy-D-lyxo-hex-1-enitol

: 944064-71-5
C₆₉H₉₄N₂SiO₁₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: 75 percent / tin (II) triflate / CH₂Cl₂; acetonitrile / 0 °C

2.1: sodium methanolate / methanol

3.1: 1.4 g / sodium hydride / dimethylformamide / 16 h

4.1: conc. nitric acid; acetic anhydride / CH₂Cl₂ / 1 h / -30 °C

4.2: 68 percent / triethylamine / CH₂Cl₂ / 0.42 h

5.1: potassium tert-butoxide / toluene / 2 h

With potassium tert-butylate; nitric acid; sodium methylate; acetic anhydride; sodium hydride; tin (II) triflate; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/jo061670b

Reference yield:

: C₄₂H₅₈SiO₉

: 944064-71-5
C₆₉H₉₄N₂SiO₁₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1.4 g / sodium hydride / dimethylformamide / 16 h

2.1: conc. nitric acid; acetic anhydride / CH₂Cl₂ / 1 h / -30 °C

2.2: 68 percent / triethylamine / CH₂Cl₂ / 0.42 h

3.1: potassium tert-butoxide / toluene / 2 h

With potassium tert-butylate; nitric acid; acetic anhydride; sodium hydride; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo061670b