N-Fmoc-L-prolyl-L-alanyl trityl sulfide

Base Information

Chemical Name:N-Fmoc-L-prolyl-L-alanyl trityl sulfide
CAS No.:1333014-04-2
Molecular Formula:C₄₂H₃₈N₂O₄S
Molecular Weight:666.841
Hs Code.:

Synonyms:N-Fmoc-L-prolyl-L-alanyl trityl sulfide

Suppliers and Price of N-Fmoc-L-prolyl-L-alanyl trityl sulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Fmoc-L-prolyl-L-alanyl trityl sulfide

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Technology Process of N-Fmoc-L-prolyl-L-alanyl trityl sulfide

There total 2 articles about N-Fmoc-L-prolyl-L-alanyl trityl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 144575-15-5
2-(1-carboxyethylcarbamoyl)pyrrolidine-1-carboxylic acid 1-(9H-fluoren-9-ylmethyl) ester

: 3695-77-0
triphenylmethanethiol

: 1333014-04-2
N-Fmoc-L-prolyl-L-alanyl trityl sulfide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; for 3h;
DOI:10.1021/ol202163e

Reference yield:

: 71989-31-6
Fmoc-Pro-OH

: 1333014-04-2
N-Fmoc-L-prolyl-L-alanyl trityl sulfide

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 6 h / Inert atmosphere; solid phase reaction

1.2: 4 h / 20 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 3 h

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide;
DOI:10.1021/ol202163e