C₅₈H₉₅BrO₁₀Si₂

Base Information

• Chemical Name: C₅₈H₉₅BrO₁₀Si₂
• CAS No.: 902132-77-8
• Molecular Formula: C₅₈H₉₅BrO₁₀Si₂
• Molecular Weight: 1088.46
• Mol file: 902132-77-8.mol

Synonyms:C₅₈H₉₅BrO₁₀Si₂

Chemical Property of C₅₈H₉₅BrO₁₀Si₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₈H₉₅BrO₁₀Si₂

There total 23 articles about C₅₈H₉₅BrO₁₀Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C64H107BrN2O10Si2 → C58H95BrO10Si2 (902132-77-8)

Guidance literature:

With oxalic acid; In diethyl ether; at 25 ℃; for 48h;

DOI:10.1039/b602020h

Reference yield:

C27H47IO4Si (902132-07-4) → C58H95BrO10Si2 (902132-77-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: LDA / tetrahydrofuran / 1 h / -78 °C

1.2: tetrahydrofuran / 1 h / -78 °C

2.1: 1.02 g / aq. (CO₂H)2 / diethyl ether / 48 h / 25 °C

With oxalic acid; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;

DOI:10.1039/b602020h

Reference yield:

C15H15BrClNO4 (902132-64-3) → C58H95BrO10Si2 (902132-77-8)

Guidance literature:

Multi-step reaction with 14 steps

1.1: 81 percent / Zn; NH₄Cl / methanol / 6 h / 25 °C

2.1: 95 percent / 2,6-lutidine / CH₂Cl₂ / 2 h / 0 - 25 °C

3.1: 85 percent / LiBH₄ / tetrahydrofuran; methanol / 3 h / -78 - 0 °C

4.1: 89 percent / NaHCO₃; Dess-Martin periodinane / CH₂Cl₂; dimethylsulfoxide / 1.5 h / 25 °C

5.1: BF₃*Et₂O / tetrahydrofuran; hexane / 0.5 h / -78 °C

5.2: tetrahydrofuran; hexane / 3 h / -78 °C

5.3: 1.123 g / aq. H₂O₂; NaOH / methanol; tetrahydrofuran; hexane / 16 h / 0 - 25 °C

6.1: Ph₃CBF₄ / diethyl ether / 18 h / 25 °C

7.1: O₃ / CH₂Cl₂ / -78 °C

7.2: PPh₃ / CH₂Cl₂ / 1 h / -78 - 25 °C

8.1: 0.908 g / benzene / 16 h / 80 °C

9.1: 87 percent / DIBAL-H / toluene / 1 h / 0 °C

10.1: Et₃N / tetrahydrofuran / 1 h / 0 °C

11.1: 2.888 g / LiBr / tetrahydrofuran / 0.5 h / 25 °C

12.1: LDA / tetrahydrofuran / 2.5 h / -78 °C

12.2: 91 percent / tetrahydrofuran / 1 h / -78 °C

13.1: LDA / tetrahydrofuran / 1 h / -78 °C

13.2: tetrahydrofuran / 1 h / -78 °C

14.1: 1.02 g / aq. (CO₂H)2 / diethyl ether / 48 h / 25 °C

With 2,6-dimethylpyridine; lithium borohydride; boron trifluoride diethyl etherate; trityl tetrafluoroborate; oxalic acid; diisobutylaluminium hydride; sodium hydrogencarbonate; ammonium chloride; Dess-Martin periodane; ozone; triethylamine; lithium bromide; zinc; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; toluene; benzene; 5.2: Brown crotylboration / 8.1: Wittig olefination;

DOI:10.1039/b602020h

upstream raw materials:

C₂₇H₄₇IO₄Si

C₁₅H₁₅BrClNO₄

C₁₅H₁₆BrNO₄

C₂₁H₃₀BrNO₄Si