3-benzyl-4-phenylbutanal

Base Information

Chemical Name:3-benzyl-4-phenylbutanal
CAS No.:93651-34-4
Molecular Formula:C₁₇H₁₈O
Molecular Weight:238.329
Hs Code.:

Synonyms:3-benzyl-4-phenylbutanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-benzyl-4-phenylbutanal

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Technology Process of 3-benzyl-4-phenylbutanal

There total 7 articles about 3-benzyl-4-phenylbutanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 3,3-dibenzyl-1-propanol

: 93651-34-4
3-benzyl-4-phenylbutanal

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In dichloromethane; at 25 ℃; for 2h; Molecular sieve; Inert atmosphere;
DOI:10.1039/c9cc00223e

Reference yield:

: 198547-74-9
ethyl 3-benzyl-4-phenylbut-2-enoate

: 93651-34-4
3-benzyl-4-phenylbutanal

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 25 °C / 760.05 Torr

2: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 - 25 °C / Inert atmosphere

3: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 2 h / 25 °C / Molecular sieve; Inert atmosphere

With lithium aluminium tetrahydride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; palladium 10% on activated carbon; hydrogen; In methanol; diethyl ether; dichloromethane;
DOI:10.1039/c9cc00223e

Reference yield:

: 781-35-1
1,1-diphenylacetone

: 93651-34-4
3-benzyl-4-phenylbutanal

Guidance literature:: Multi-step reaction with 4 steps

1: benzene / 12 h / 100 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 25 °C / 760.05 Torr

3: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 - 25 °C / Inert atmosphere

4: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 2 h / 25 °C / Molecular sieve; Inert atmosphere

With lithium aluminium tetrahydride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; palladium 10% on activated carbon; hydrogen; In methanol; diethyl ether; dichloromethane; benzene; 1: |Wittig Olefination;
DOI:10.1039/c9cc00223e